1-(3-mesitylimidazolium)-15-(2-hydroxyphenyl)-4,5-dibenzo-3,6,9,12,15-pentaoxapentadecane chloride

Base Information

Chemical Name:1-(3-mesitylimidazolium)-15-(2-hydroxyphenyl)-4,5-dibenzo-3,6,9,12,15-pentaoxapentadecane chloride
CAS No.:1396365-62-0
Molecular Formula:C₃₂H₃₉N₂O₆*Cl
Molecular Weight:583.124
Hs Code.:

Synonyms:1-(3-mesitylimidazolium)-15-(2-hydroxyphenyl)-4,5-dibenzo-3,6,9,12,15-pentaoxapentadecane chloride

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Chemical Property of 1-(3-mesitylimidazolium)-15-(2-hydroxyphenyl)-4,5-dibenzo-3,6,9,12,15-pentaoxapentadecane chloride

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Technology Process of 1-(3-mesitylimidazolium)-15-(2-hydroxyphenyl)-4,5-dibenzo-3,6,9,12,15-pentaoxapentadecane chloride

There total 3 articles about 1-(3-mesitylimidazolium)-15-(2-hydroxyphenyl)-4,5-dibenzo-3,6,9,12,15-pentaoxapentadecane chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1-mesitylimidazole

: 1396365-57-3
1-chloro-15-(2-hydroxyphenyl)-4,5-dibenzo-3,9,12,15-pentaoxapentadecane

: 1396365-62-0
1-(3-mesitylimidazolium)-15-(2-hydroxyphenyl)-4,5-dibenzo-3,6,9,12,15-pentaoxapentadecane chloride

Guidance literature:: In 5,5-dimethyl-1,3-cyclohexadiene; at 150 ℃; for 50h; Inert atmosphere;
DOI:10.1002/cjoc.201100596

Reference yield:

: 1396365-54-0
1-hydroxy-15-(2-hydroxyphenyl)-4,5-dibenzo-3,6,9,12,15-pentaoxapentadecane

: 1396365-62-0
1-(3-mesitylimidazolium)-15-(2-hydroxyphenyl)-4,5-dibenzo-3,6,9,12,15-pentaoxapentadecane chloride

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; thionyl chloride / benzene / 8 h / 80 °C / Inert atmosphere

2: 5,5-dimethyl-1,3-cyclohexadiene / 50 h / 150 °C / Inert atmosphere

With pyridine; thionyl chloride; In 5,5-dimethyl-1,3-cyclohexadiene; benzene;
DOI:10.1002/cjoc.201100596

Reference yield:

: 68822-97-9
1,8-bis(2-hydroxyphenoxy)-3,6-dioxaoctane

: 1396365-62-0
1-(3-mesitylimidazolium)-15-(2-hydroxyphenyl)-4,5-dibenzo-3,6,9,12,15-pentaoxapentadecane chloride

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / tert-butyl alcohol / 24 h / Reflux; Inert atmosphere

2: pyridine; thionyl chloride / benzene / 8 h / 80 °C / Inert atmosphere

3: 5,5-dimethyl-1,3-cyclohexadiene / 50 h / 150 °C / Inert atmosphere

With pyridine; thionyl chloride; sodium hydroxide; In 5,5-dimethyl-1,3-cyclohexadiene; tert-butyl alcohol; benzene;
DOI:10.1002/cjoc.201100596