2-(2-Methylamino-benzenesulfinyl)-cycloundecanone

Base Information

Chemical Name:2-(2-Methylamino-benzenesulfinyl)-cycloundecanone
CAS No.:87054-21-5
Molecular Formula:C₁₈H₂₇NO₂S
Molecular Weight:321.484
Hs Code.:

Synonyms:2-(2-Methylamino-benzenesulfinyl)-cycloundecanone

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Chemical Property of 2-(2-Methylamino-benzenesulfinyl)-cycloundecanone

Chemical Property:

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Technology Process of 2-(2-Methylamino-benzenesulfinyl)-cycloundecanone

There total 8 articles about 2-(2-Methylamino-benzenesulfinyl)-cycloundecanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15949-84-5
11-bromoundecanoyl chloride

: 87054-21-5
2-(2-Methylamino-benzenesulfinyl)-cycloundecanone

Guidance literature:: Multi-step reaction with 4 steps

1: 10 percent / Et₃N / diethyl ether / 0.5 h / Ambient temperature

2: 84.4 percent / NaBH₄, NaH, 2-propanol / dioxane / 1.) 70 deg C, 2.) reflux, 1 h

3: 94 percent / NaIO₄ / H₂O; methanol / 20 h / Ambient temperature

4: LDA / tetrahydrofuran / 1.) -78 deg C, 30 min, 2.) 30 min, ice bath

With sodium tetrahydroborate; sodium periodate; sodium hydride; triethylamine; isopropyl alcohol; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; water;

Reference yield:

: 3495-63-4
2,2'-dithiobis(N-methylaniline)

: 87054-21-5
2-(2-Methylamino-benzenesulfinyl)-cycloundecanone

Guidance literature:: Multi-step reaction with 4 steps

1: 10 percent / Et₃N / diethyl ether / 0.5 h / Ambient temperature

2: 84.4 percent / NaBH₄, NaH, 2-propanol / dioxane / 1.) 70 deg C, 2.) reflux, 1 h

3: 94 percent / NaIO₄ / H₂O; methanol / 20 h / Ambient temperature

4: LDA / tetrahydrofuran / 1.) -78 deg C, 30 min, 2.) 30 min, ice bath

With sodium tetrahydroborate; sodium periodate; sodium hydride; triethylamine; isopropyl alcohol; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; water;

Reference yield:

: 2834-05-1
11-bromoundecanoic acid

: 87054-21-5
2-(2-Methylamino-benzenesulfinyl)-cycloundecanone

Guidance literature:: Multi-step reaction with 5 steps

1: SOCl₂ / 3 h / Heating

2: 10 percent / Et₃N / diethyl ether / 0.5 h / Ambient temperature

3: 84.4 percent / NaBH₄, NaH, 2-propanol / dioxane / 1.) 70 deg C, 2.) reflux, 1 h

4: 94 percent / NaIO₄ / H₂O; methanol / 20 h / Ambient temperature

5: LDA / tetrahydrofuran / 1.) -78 deg C, 30 min, 2.) 30 min, ice bath

With sodium tetrahydroborate; sodium periodate; thionyl chloride; sodium hydride; triethylamine; isopropyl alcohol; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; water;