4-[3-(7-chloro-4-oxo-1-phenyl-1,4-dihydro-quinolin-3-ylmethyl)ureido]piperidine-1-carboxylic acid 4-nitrophenyl ester

Base Information

Chemical Name:4-[3-(7-chloro-4-oxo-1-phenyl-1,4-dihydro-quinolin-3-ylmethyl)ureido]piperidine-1-carboxylic acid 4-nitrophenyl ester
CAS No.:1418026-27-3
Molecular Formula:C₂₉H₂₆ClN₅O₆
Molecular Weight:576.008
Hs Code.:

Synonyms:4-[3-(7-chloro-4-oxo-1-phenyl-1,4-dihydro-quinolin-3-ylmethyl)ureido]piperidine-1-carboxylic acid 4-nitrophenyl ester

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Chemical Property of 4-[3-(7-chloro-4-oxo-1-phenyl-1,4-dihydro-quinolin-3-ylmethyl)ureido]piperidine-1-carboxylic acid 4-nitrophenyl ester

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Technology Process of 4-[3-(7-chloro-4-oxo-1-phenyl-1,4-dihydro-quinolin-3-ylmethyl)ureido]piperidine-1-carboxylic acid 4-nitrophenyl ester

There total 12 articles about 4-[3-(7-chloro-4-oxo-1-phenyl-1,4-dihydro-quinolin-3-ylmethyl)ureido]piperidine-1-carboxylic acid 4-nitrophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1418026-15-9
1-(7-chloro-4-oxo-1-phenyl-1,4-dihydro-quinolin-3-ylmethyl)-3-piperidin-4-yl-urea hydrochloride

: 7693-46-1
4-Nitrophenyl chloroformate

: 1418026-27-3
4-[3-(7-chloro-4-oxo-1-phenyl-1,4-dihydro-quinolin-3-ylmethyl)ureido]piperidine-1-carboxylic acid 4-nitrophenyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; under 760.051 Torr; Inert atmosphere;

Reference yield:

: 1418026-14-8
(7-chloro-4-oxo-1-phenyl-1,4-dihydro-quinolin-3-ylmethyl)carbamic acid 4-nitro-phenyl ester

: 1418026-27-3
4-[3-(7-chloro-4-oxo-1-phenyl-1,4-dihydro-quinolin-3-ylmethyl)ureido]piperidine-1-carboxylic acid 4-nitrophenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / 760.05 Torr / Inert atmosphere

2: hydrogenchloride / 1,4-dioxane / 20 °C / 760.05 Torr / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / 760.05 Torr / Inert atmosphere

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane;

Reference yield:

: 1418025-47-4
4-[3-(7-chloro-4-oxo-1-phenyl-1,4-dihydro-quinolin-3-ylmethyl)ureido]piperidine-1-carboxylic acid tert-butyl ester

: 1418026-27-3
4-[3-(7-chloro-4-oxo-1-phenyl-1,4-dihydro-quinolin-3-ylmethyl)ureido]piperidine-1-carboxylic acid 4-nitrophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / 1,4-dioxane / 20 °C / 760.05 Torr / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / 760.05 Torr / Inert atmosphere

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane;