C₇₄H₉₁N₈O₉⁽¹⁺⁾*Cl^(1-)

Base Information

• Chemical Name: C₇₄H₉₁N₈O₉⁽¹⁺⁾*Cl^(1-)
• CAS No.: 1616283-00-1
• Molecular Formula: C₇₄H₉₁N₈O₉*Cl
• Molecular Weight: 1272.04
• Mol file: 1616283-00-1.mol

Synonyms:C₇₄H₉₁N₈O₉⁽¹⁺⁾*Cl^(1-)

Chemical Property of C₇₄H₉₁N₈O₉⁽¹⁺⁾*Cl^(1-)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₇₄H₉₁N₈O₉⁽¹⁺⁾*Cl^(1-)

There total 6 articles about C₇₄H₉₁N₈O₉⁽¹⁺⁾*Cl^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

1-methyl-1H-imidazole (616-47-7) + C70H85ClN6O9 (1616282-99-5) → C74H91N8O9(1+)*Cl(1-) (1616283-00-1)

Guidance literature:

In toluene; at 80 ℃; Inert atmosphere;

DOI:10.1021/ja5041573

Reference yield:

8-bromooctanol (50816-19-8) → C74H91N8O9(1+)*Cl(1-) (1616283-00-1)

Guidance literature:

Multi-step reaction with 6 steps

1: potassium carbonate / N,N-dimethyl-formamide / 14 h / 80 °C / Inert atmosphere

2: phosphorus tribromide / N,N-dimethyl-formamide; dichloromethane; tetrahydrofuran / 20 °C / Inert atmosphere

3: potassium carbonate / N,N-dimethyl-formamide / 12 h / 70 °C / Inert atmosphere

4: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C / Inert atmosphere

5: thionyl chloride / dichloromethane / 0 - 20 °C / Inert atmosphere

6: toluene / 80 °C / Inert atmosphere

With lithium aluminium tetrahydride; thionyl chloride; phosphorus tribromide; potassium carbonate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;

DOI:10.1021/ja5041573

Reference yield:

C21H28N2O3 (1575790-50-9) → C74H91N8O9(1+)*Cl(1-) (1616283-00-1)

Guidance literature:

Multi-step reaction with 5 steps

1: phosphorus tribromide / N,N-dimethyl-formamide; dichloromethane; tetrahydrofuran / 20 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 12 h / 70 °C / Inert atmosphere

3: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C / Inert atmosphere

4: thionyl chloride / dichloromethane / 0 - 20 °C / Inert atmosphere

5: toluene / 80 °C / Inert atmosphere

With lithium aluminium tetrahydride; thionyl chloride; phosphorus tribromide; potassium carbonate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;

DOI:10.1021/ja5041573

upstream raw materials:

C₇₁H₈₆N₆O₁₁

1-methyl-1H-imidazole

C₇₀H₈₅ClN₆O₉

(E)-4-hydroxy-4′-methoxyazobenzene

Refernces