Mes₂BOMe

Base Information Edit

Chemical Name:Mes₂BOMe
CAS No.:50517-71-0
Molecular Formula:C₁₉H₂₅BO
Molecular Weight:280.218
Hs Code.:
Mol file:50517-71-0.mol

Synonyms:Mes₂BOMe

Suppliers and Price of Mes₂BOMe

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Mes₂BOMe Edit

Chemical Property:

Purity/Quality:

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Technology Process of Mes₂BOMe

There total 5 articles about Mes₂BOMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 121-43-7,63156-11-6
Trimethyl borate

: 2633-66-1
2-mesitylmagnesium bromide

: 50517-71-0
Mes₂BOMe

Guidance literature:: In tetrahydrofuran; at 55 ℃; for 5h; Inert atmosphere; Schlenk technique;
DOI:10.1002/zaac.201900313

Reference yield: 65.0%

: 121-43-7,63156-11-6
Trimethyl borate

: 576-83-0
2,4,6-trimethylphenyl bromide

: 50517-71-0
Mes₂BOMe

Guidance literature:: 2,4,6-trimethylphenyl bromide; With magnesium; In tetrahydrofuran; ethylene dibromide; for 3h; Inert atmosphere; Reflux;

Trimethyl borate; In tetrahydrofuran; ethylene dibromide; at 20 ℃; for 12h; Cooling with ice;

Reference yield:

: 82945-06-0
bis(dimesitylboryl)methane

: 50517-71-0
Mes₂BOMe

: 74178-56-6
methyl(dimesityl)borane

Guidance literature:: With methanol; In tetrahydrofuran; slight excess of MeOH, stirred overnight, solvent was removed under high vac.; detected by (1)H NMR;