methyl(dimesityl)borane

Base Information

• Chemical Name: methyl(dimesityl)borane
• CAS No.: 74178-56-6
• Molecular Formula: C₁₉H₂₅B
• Molecular Weight: 264.218
• Mol file: 74178-56-6.mol

Synonyms:methyl(dimesityl)borane

Chemical Property of methyl(dimesityl)borane

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl(dimesityl)borane

There total 7 articles about methyl(dimesityl)borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

dimesitylfluoroborane (436-59-9) → methyl(dimesityl)borane (74178-56-6)

Guidance literature:

In not given; (N2); react. of borane and appropriate Grignard reagent according to P.Finocchiaro, D. Gust and K. Mislow, J. Amer. Chem. Soc., 95 (1973) 7029; elem. anal.;

DOI:10.1016/S0022-328X(00)82409-2

Reference yield:

bis(dimesitylboryl)methane (82945-06-0) → (C6H2(CH3)3)2BOCH2CH3 (75260-09-2) + methyl(dimesityl)borane (74178-56-6)

Guidance literature:

With CH₃H₂OH; In tetrahydrofuran; slight excess of EtOH, stirred overnight, solvent was removed under high vac.; detected by (1)H NMR;

Reference yield:

bis(dimesitylboryl)methane (82945-06-0) → (C6H2(CH3)3)2BOC6H5 (75260-16-1) + methyl(dimesityl)borane (74178-56-6)

Guidance literature:

With phenol; In tetrahydrofuran; slight excess of C6H5OH, stirred overnight, solvent was removed under high vac.; detected by (1)H NMR;

upstream raw materials:

dimesitylfluoroborane

bis(dimesitylboryl)methane

water

isobutylamine

Downstream raw materials:

Mesitol

nonyl alcohol

2-phenylethanol

dimesitylethylborane