methyl 2-(trifluoroacetamido)-5-<(tert-butyldimethylsilyl)oxy>benzoate

Base Information

Chemical Name:methyl 2-(trifluoroacetamido)-5-<(tert-butyldimethylsilyl)oxy>benzoate
CAS No.:135006-38-1
Molecular Formula:C₁₆H₂₂F₃NO₄Si
Molecular Weight:377.436
Hs Code.:

Synonyms:methyl 2-(trifluoroacetamido)-5-<(tert-butyldimethylsilyl)oxy>benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-(trifluoroacetamido)-5-<(tert-butyldimethylsilyl)oxy>benzoate

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Technology Process of methyl 2-(trifluoroacetamido)-5-<(tert-butyldimethylsilyl)oxy>benzoate

There total 1 articles about methyl 2-(trifluoroacetamido)-5-<(tert-butyldimethylsilyl)oxy>benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 72297-76-8
5-Hydroxy-2-(2,2,2-trifluoro-acetylamino)-benzoic acid methyl ester

: 18162-48-6
tert-butyldimethylsilyl chloride

: 135006-38-1
methyl 2-(trifluoroacetamido)-5-<(tert-butyldimethylsilyl)oxy>benzoate

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 16h; Ambient temperature;

Reference yield: 98.0%

: 135006-38-1
methyl 2-(trifluoroacetamido)-5-<(tert-butyldimethylsilyl)oxy>benzoate

: 74-88-4
methyl iodide

: 135006-39-2
methyl 2-(N-methyltrifluoroacetamido)-5-<(tert-butyldimethylsilyl)oxy>benzoate

Guidance literature:: With potassium carbonate; In acetone; at 50 ℃; for 5h;

Reference yield:

: 135006-38-1
methyl 2-(trifluoroacetamido)-5-<(tert-butyldimethylsilyl)oxy>benzoate

: 135006-41-6
methyl 5-hydroxy-2-(N-methyltrifluoroacetamido)-4-nitrobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / K₂CO₃ / acetone / 5 h / 50 °C

2: conc. aq. HF, conc. aq. HNO₃ / nitromethane / 1.5 h / Ambient temperature

With hydrogen fluoride; nitric acid; potassium carbonate; In nitromethane; acetone;