3,6-anhydro-1,2-O-(1-methylethylidene)-5-O-[(4-methylphenyl)sulfonyl]hexofuranose

Base Information

• Chemical Name: 3,6-anhydro-1,2-O-(1-methylethylidene)-5-O-[(4-methylphenyl)sulfonyl]hexofuranose
• CAS No.: 2592-47-4
• Molecular Formula: C₁₆H₂₀O₇S
• Molecular Weight: 356.397

Synonyms:3,6-anhydro-1,2-O-isopropylidene-5-O-toluene-p-sulfonyl-α-D-glucofuranose

Chemical Property of 3,6-anhydro-1,2-O-(1-methylethylidene)-5-O-[(4-methylphenyl)sulfonyl]hexofuranose

Chemical Property:

• Vapor Pressure: 4.38E-09mmHg at 25°C
• Melting Point: 133-135 °C
• Boiling Point: 484.9±45.0 °C(Predicted)
• Density: 1.42±0.1 g/cm3(Predicted)

Purity/Quality:

Safty Information:

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Technology Process of 3,6-anhydro-1,2-O-(1-methylethylidene)-5-O-[(4-methylphenyl)sulfonyl]hexofuranose

There total 5 articles about 3,6-anhydro-1,2-O-(1-methylethylidene)-5-O-[(4-methylphenyl)sulfonyl]hexofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

O1,O2-isopropylidene-O5,O6-bis-(toluene-4-sulfonyl)-α-D-glucofuranose (6935-51-9) → 3,6-anhydro-1,2-O-isopropylidene-5-O-toluene-p-sulfonyl-α-D-glucofuranose (2592-47-4)

Guidance literature:

With sodium hydroxide;

Reference yield:

ethanol (64-17-5) + O1,O2-isopropylidene-O5,O6-bis-(toluene-4-sulfonyl)-α-D-glucofuranose (6935-51-9) → 3,6-anhydro-1,2-O-isopropylidene-5-O-toluene-p-sulfonyl-α-D-glucofuranose (2592-47-4)

Guidance literature:

DOI:10.1021/ja01181a080

Reference yield:

O1,O2-isopropylidene-O5,O6-bis-(toluene-4-sulfonyl)-α-D-glucofuranose (6935-51-9) → 3,6-anhydro-1,2-O-isopropylidene-5-O-toluene-p-sulfonyl-α-D-glucofuranose (2592-47-4)

Guidance literature:

upstream raw materials:

O¹,O²-isopropylidene-O⁵,O⁶-bis-(toluene-4-sulfonyl)-α-D-glucofuranose

chloroform

p-toluenesulfonyl chloride

1,2-O-isopropylidene-α-D-glucofuranose

Downstream raw materials:

3,6-anhydro-5-deoxy-1,2-O-isopropylidene-α-D-xylo-hex-5-enofuranose

3,6-Anhydro-5-desoxy-5-iod-1,2-O-isopropyliden-β-L-idofuranose

3,6-anhydro-5-deoxy-1,2-O-isopropylidene-α-D-erythro-hex-4-enofuranose

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