epi-5-deoxy-5-(2-aminoethyl)amino-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetylneamine

Base Information

Chemical Name:epi-5-deoxy-5-(2-aminoethyl)amino-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetylneamine
CAS No.:1432025-39-2
Molecular Formula:C₂₀H₃₀N₁₄O₈
Molecular Weight:594.547
Hs Code.:

Synonyms:epi-5-deoxy-5-(2-aminoethyl)amino-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetylneamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of epi-5-deoxy-5-(2-aminoethyl)amino-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetylneamine

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Technology Process of epi-5-deoxy-5-(2-aminoethyl)amino-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetylneamine

There total 3 articles about epi-5-deoxy-5-(2-aminoethyl)amino-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetylneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₂₃F₃N₁₂O₁₁S

: 107-15-3,85404-18-8
ethylenediamine

: 1432025-39-2
epi-5-deoxy-5-(2-aminoethyl)amino-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetylneamine

Guidance literature:: With pyridine; In acetonitrile; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.cclet.2013.03.009

Reference yield:

: 236115-80-3
1,3,2',6'-tetraazido-6,3',4'-tri-O-benzyl neamine

: 1432025-39-2
epi-5-deoxy-5-(2-aminoethyl)amino-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetylneamine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 6 h / 20 °C / Inert atmosphere

2: pyridine / acetonitrile / 0.5 h / 20 °C / Inert atmosphere

With pyridine; In dichloromethane; acetonitrile;
DOI:10.1016/j.cclet.2013.03.009

Reference yield:

: 182554-04-7
1,3,2′,6′-tetraazido-6,3′,4′-tri-O-acetylneamine

: 1432025-39-2
epi-5-deoxy-5-(2-aminoethyl)amino-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetylneamine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 3.5 h / 20 °C / Inert atmosphere

2: pyridine / acetonitrile / 0.5 h / 20 °C / Inert atmosphere

With pyridine; In dichloromethane; acetonitrile;
DOI:10.1016/j.cclet.2013.03.009