9-(4-fluorophenyl)-9H-carbazol-3-amine

Base Information

Chemical Name:9-(4-fluorophenyl)-9H-carbazol-3-amine
CAS No.:1454710-62-3
Molecular Formula:C₁₈H₁₃FN₂
Molecular Weight:276.313
Hs Code.:

Synonyms:9-(4-fluorophenyl)-9H-carbazol-3-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-(4-fluorophenyl)-9H-carbazol-3-amine

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Technology Process of 9-(4-fluorophenyl)-9H-carbazol-3-amine

There total 3 articles about 9-(4-fluorophenyl)-9H-carbazol-3-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1454710-53-2
9-(4-fluorophenyl)-3-nitro-9H-carbazole

: 1454710-62-3
9-(4-fluorophenyl)-9H-carbazol-3-amine

Guidance literature:: With palladium 10% on activated carbon; hydrazine hydrate; In tetrahydrofuran; methanol; ethanol; at 60 ℃; for 1.08333h;
DOI:10.1016/j.tet.2013.07.040

Reference yield:

: 86-74-8,105184-46-1,97960-57-1
9H-carbazole

: 1454710-62-3
9-(4-fluorophenyl)-9H-carbazol-3-amine

Guidance literature:: Multi-step reaction with 3 steps

1: copper nitrate hemi(pentahydrate); acetic acid; acetic anhydride / 0.75 h / 60 °C

2: potassium carbonate / 8 h / 180 °C

3: hydrazine hydrate; palladium 10% on activated carbon / tetrahydrofuran; ethanol; methanol / 1.08 h / 60 °C

With copper nitrate hemi(pentahydrate); palladium 10% on activated carbon; acetic anhydride; potassium carbonate; hydrazine hydrate; acetic acid; In tetrahydrofuran; methanol; ethanol;
DOI:10.1016/j.tet.2013.07.040

Reference yield:

: 3077-85-8
3-Nitro-carbazol

: 1454710-62-3
9-(4-fluorophenyl)-9H-carbazol-3-amine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / 8 h / 180 °C

2: hydrazine hydrate; palladium 10% on activated carbon / tetrahydrofuran; ethanol; methanol / 1.08 h / 60 °C

With palladium 10% on activated carbon; potassium carbonate; hydrazine hydrate; In tetrahydrofuran; methanol; ethanol;
DOI:10.1016/j.tet.2013.07.040