iron(2+) cyclopenta-2,4-dienide 3-(3-oxo-3-phenylprop-1-en-1-yl)cyclopenta-2,4-dienide (1:1:1)

Base Information

Chemical Name:iron(2+) cyclopenta-2,4-dienide 3-(3-oxo-3-phenylprop-1-en-1-yl)cyclopenta-2,4-dienide (1:1:1)
CAS No.:6318-84-9
Molecular Formula:C19H16FeO
Molecular Weight:316.182
Hs Code.:

Synonyms:

Suppliers and Price of iron(2+) cyclopenta-2,4-dienide 3-(3-oxo-3-phenylprop-1-en-1-yl)cyclopenta-2,4-dienide (1:1:1)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of iron(2+) cyclopenta-2,4-dienide 3-(3-oxo-3-phenylprop-1-en-1-yl)cyclopenta-2,4-dienide (1:1:1)

Chemical Property:

Vapor Pressure:0.000105mmHg at 25°C
Boiling Point:337.4°C at 760 mmHg
Flash Point:146°C

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of iron(2+) cyclopenta-2,4-dienide 3-(3-oxo-3-phenylprop-1-en-1-yl)cyclopenta-2,4-dienide (1:1:1)

There total 8 articles about iron(2+) cyclopenta-2,4-dienide 3-(3-oxo-3-phenylprop-1-en-1-yl)cyclopenta-2,4-dienide (1:1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 12093-10-6
ferrocenecarboxaldehyde

: 98-86-2
acetophenone

: 6318-84-9
3-ferrocenyl-1-phenylprop-2-en-1-one

Guidance literature:: With potassium hydroxide; In ethanol; water; aldehyde added to an ethanol soln. of the methylketone and 10% aq. KOH, mixt. stirred, room temp., 2 h; ppt. filtered, recrystd. from CH3OH;
DOI:10.1246/bcsj.63.3710

Reference yield: 86.0%

: 1273-86-5
1-ferrocenylmethanol

: 98-85-1,13323-81-4
1-Phenylethanol

: 6318-84-9
3-ferrocenyl-1-phenylprop-2-en-1-one

Guidance literature:: With [Ni(dmpymt)₂]₆; potassium hydroxide; In toluene; tert-butyl alcohol; at 70 ℃; for 36h; chemoselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1039/C9OB00418A

Reference yield: 71.0%

: 12093-10-6
ferrocenecarboxaldehyde

: 6048-29-9
triphenylphenacylphosphonium bromide

: 6318-84-9
3-ferrocenyl-1-phenylprop-2-en-1-one

Guidance literature:: With sodium hydroxide; In solid; thorough grounding a mixt. of aldehyde and phosphonium salt with NaOH atroom temp., heating at 65°C for 240 min, grounding for 1-2 min, cooling to room temp.; extn. with CH2Cl2, drying with Na2SO4, filtration, evapn., chromy (SiO2,petroleum ether);
DOI:10.1016/S0022-328X(00)00927-X