2-{1-[(2-aminoethyl)amino]-2-phenylethylidene}-5,5-dimethyl-1,3-cyclohexanedione

Base Information

Chemical Name:2-{1-[(2-aminoethyl)amino]-2-phenylethylidene}-5,5-dimethyl-1,3-cyclohexanedione
CAS No.:623929-46-4
Molecular Formula:C₁₈H₂₄N₂O₂
Molecular Weight:300.401
Hs Code.:

Synonyms:2-{1-[(2-aminoethyl)amino]-2-phenylethylidene}-5,5-dimethyl-1,3-cyclohexanedione

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Chemical Property of 2-{1-[(2-aminoethyl)amino]-2-phenylethylidene}-5,5-dimethyl-1,3-cyclohexanedione

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Technology Process of 2-{1-[(2-aminoethyl)amino]-2-phenylethylidene}-5,5-dimethyl-1,3-cyclohexanedione

There total 1 articles about 2-{1-[(2-aminoethyl)amino]-2-phenylethylidene}-5,5-dimethyl-1,3-cyclohexanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 107-15-3,85404-18-8
ethylenediamine

: 204777-75-3
2-(1-hydroxy-2-phenylethylidene)-5,5-dimethylcyclohexane-1,3-dione

: 623929-46-4
2-{1-[(2-aminoethyl)amino]-2-phenylethylidene}-5,5-dimethyl-1,3-cyclohexanedione

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 36h;
DOI:10.1021/jo0348874

Reference yield: 69.0%

: 137743-46-5
2-tert-butyloxycarbonylaminoethyl isothiocyanate

: 623929-46-4
2-{1-[(2-aminoethyl)amino]-2-phenylethylidene}-5,5-dimethyl-1,3-cyclohexanedione

: 623929-50-0
[2-(3-{2-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-2-phenylethylamino]ethyl}thioureido)ethyl]carbamic acid tert-butyl ester

Guidance literature:: In methanol; dichloromethane; at 20 ℃; for 48h;
DOI:10.1021/jo0348874

Reference yield:

: 623929-46-4
2-{1-[(2-aminoethyl)amino]-2-phenylethylidene}-5,5-dimethyl-1,3-cyclohexanedione

: 623929-56-6
{2-[N'-{2-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-2-phenylethylamino]ethyl}-N''-(2,2,2-trifluoroacetyl)guanidino]ethyl}carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 69 percent / methanol; CH₂Cl₂ / 48 h / 20 °C

2: acetone / 18 h / 20 °C

3: ammonium hexafluorophosphate / CH₂Cl₂; methanol / 18 h / 20 °C

4: 31 mg / DBU / toluene; CHCl₃ / Heating

With ammonium hexafluorophosphate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; dichloromethane; chloroform; acetone; toluene;
DOI:10.1021/jo0348874