Technology Process of C29H32ClN7O10S2
There total 7 articles about C29H32ClN7O10S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C71H75ClN7O15S2(1+)*I(1-);
With
aluminum (III) chloride;
In
nitromethane; dichloromethane; methoxybenzene;
at -40 - 0 ℃;
for 1h;
With
hydrogenchloride;
In
nitromethane; dichloromethane; di-isopropyl ether; water; methoxybenzene; acetonitrile;
- Guidance literature:
-
2-chloro-3,4-bis((4-methoxybenzyl)oxy)-N-(2-(pyrrolidin-1-yl)ethyl)benzamide; C42H42IN5O11S2;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 3.5h;
Inert atmosphere;
With
acetyl chloride; potassium iodide;
In
N,N-dimethyl-formamide;
at 0 ℃;
for 1h;
Inert atmosphere;
With
aluminum (III) chloride; methoxybenzene;
In
nitromethane; dichloromethane;
at -40 - 0 ℃;
for 1.33333h;
Inert atmosphere;
DOI:10.1016/j.ejmech.2018.06.014
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: boron tribromide / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere
1.2: Inert atmosphere
2.1: potassium carbonate; sodium iodide / N,N-dimethyl-formamide / 3.5 h / 50 °C / Inert atmosphere
3.1: sodium hydroxide / tetrahydrofuran; methanol / 1.5 h / Reflux; Inert atmosphere
4.1: triethylamine; methanesulfonyl chloride / N,N-dimethyl-formamide / 0.5 h / -10 °C / Inert atmosphere
4.2: 1 h / 0 °C / Inert atmosphere
5.1: N,N-dimethyl-formamide / 3.5 h / 20 °C / Inert atmosphere
5.2: 1 h / 0 °C / Inert atmosphere
5.3: 1.33 h / -40 - 0 °C / Inert atmosphere
With
boron tribromide; potassium carbonate; methanesulfonyl chloride; triethylamine; sodium iodide; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2018.06.014
