(2S,4S)-1-allyloxycarbonyl-2-[N-(5'-carbamoyl-1',2',4'-oxadiazol-3'-yl)methyl]carbamoyl-4-tritylthiopyrrolidine

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Chemical Name:(2S,4S)-1-allyloxycarbonyl-2-[N-(5'-carbamoyl-1',2',4'-oxadiazol-3'-yl)methyl]carbamoyl-4-tritylthiopyrrolidine
CAS No.:786720-39-6
Molecular Formula:C₃₂H₃₁N₅O₅S
Molecular Weight:597.695
Hs Code.:

Synonyms:(2S,4S)-1-allyloxycarbonyl-2-[N-(5'-carbamoyl-1',2',4'-oxadiazol-3'-yl)methyl]carbamoyl-4-tritylthiopyrrolidine

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Chemical Property of (2S,4S)-1-allyloxycarbonyl-2-[N-(5'-carbamoyl-1',2',4'-oxadiazol-3'-yl)methyl]carbamoyl-4-tritylthiopyrrolidine

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Technology Process of (2S,4S)-1-allyloxycarbonyl-2-[N-(5'-carbamoyl-1',2',4'-oxadiazol-3'-yl)methyl]carbamoyl-4-tritylthiopyrrolidine

There total 3 articles about (2S,4S)-1-allyloxycarbonyl-2-[N-(5'-carbamoyl-1',2',4'-oxadiazol-3'-yl)methyl]carbamoyl-4-tritylthiopyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.9%

: 786720-38-5
(2S,4S)-1-allyloxycarbonyl-2-[N-(5'-ethoxycarbonyl-1',2',4'-oxadiazol-3'-yl)methyl]carbamoyl-4-tritylthiopyrrolidine

: 786720-39-6
(2S,4S)-1-allyloxycarbonyl-2-[N-(5'-carbamoyl-1',2',4'-oxadiazol-3'-yl)methyl]carbamoyl-4-tritylthiopyrrolidine

Guidance literature:: With ammonium hydroxide; In ethanol; at 60 ℃; for 3h;
DOI:10.1002/ardp.200400867

Reference yield:

: 786720-32-9
(2S,4S)-1-allyloxycarbonyl-2-(N-cyanomethyl)carbamoyl-4-tritylthiopyrrolidine

: 786720-39-6
(2S,4S)-1-allyloxycarbonyl-2-[N-(5'-carbamoyl-1',2',4'-oxadiazol-3'-yl)methyl]carbamoyl-4-tritylthiopyrrolidine

Guidance literature:: Multi-step reaction with 3 steps

1: 79.6 percent / hydroxylamine hydrochloride / ethanol / 20 h / 60 °C

2: 46.2 percent / tetrahydrofuran / 12 h / Heating

3: 77.9 percent / NH₄OH / ethanol / 3 h / 60 °C

With ammonium hydroxide; hydroxylamine hydrochloride; In tetrahydrofuran; ethanol;
DOI:10.1002/ardp.200400867

Reference yield:

: 786720-37-4
(2S,4S)-1-allyloxycarbonyl-2-(N-hydroxyacetamidine)carbamoyl-4-tritylthiopyrrolidine

: 786720-39-6
(2S,4S)-1-allyloxycarbonyl-2-[N-(5'-carbamoyl-1',2',4'-oxadiazol-3'-yl)methyl]carbamoyl-4-tritylthiopyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 46.2 percent / tetrahydrofuran / 12 h / Heating

2: 77.9 percent / NH₄OH / ethanol / 3 h / 60 °C

With ammonium hydroxide; In tetrahydrofuran; ethanol;
DOI:10.1002/ardp.200400867