(2S,4S)-1-allyloxycarbonyl-2-[N-(5'-ethoxycarbonyl-1',2',4'-oxadiazol-3'-yl)methyl]carbamoyl-4-tritylthiopyrrolidine

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Chemical Name:(2S,4S)-1-allyloxycarbonyl-2-[N-(5'-ethoxycarbonyl-1',2',4'-oxadiazol-3'-yl)methyl]carbamoyl-4-tritylthiopyrrolidine
CAS No.:786720-38-5
Molecular Formula:C₃₄H₃₄N₄O₆S
Molecular Weight:626.733
Hs Code.:

Synonyms:(2S,4S)-1-allyloxycarbonyl-2-[N-(5'-ethoxycarbonyl-1',2',4'-oxadiazol-3'-yl)methyl]carbamoyl-4-tritylthiopyrrolidine

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Chemical Property of (2S,4S)-1-allyloxycarbonyl-2-[N-(5'-ethoxycarbonyl-1',2',4'-oxadiazol-3'-yl)methyl]carbamoyl-4-tritylthiopyrrolidine

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Technology Process of (2S,4S)-1-allyloxycarbonyl-2-[N-(5'-ethoxycarbonyl-1',2',4'-oxadiazol-3'-yl)methyl]carbamoyl-4-tritylthiopyrrolidine

There total 2 articles about (2S,4S)-1-allyloxycarbonyl-2-[N-(5'-ethoxycarbonyl-1',2',4'-oxadiazol-3'-yl)methyl]carbamoyl-4-tritylthiopyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.2%

: 4755-77-5
Ethyl oxalyl chloride

: 786720-37-4
(2S,4S)-1-allyloxycarbonyl-2-(N-hydroxyacetamidine)carbamoyl-4-tritylthiopyrrolidine

: 786720-38-5
(2S,4S)-1-allyloxycarbonyl-2-[N-(5'-ethoxycarbonyl-1',2',4'-oxadiazol-3'-yl)methyl]carbamoyl-4-tritylthiopyrrolidine

Guidance literature:: In tetrahydrofuran; for 12h; Heating;
DOI:10.1002/ardp.200400867

Reference yield:

: 786720-32-9
(2S,4S)-1-allyloxycarbonyl-2-(N-cyanomethyl)carbamoyl-4-tritylthiopyrrolidine

: 786720-38-5
(2S,4S)-1-allyloxycarbonyl-2-[N-(5'-ethoxycarbonyl-1',2',4'-oxadiazol-3'-yl)methyl]carbamoyl-4-tritylthiopyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 79.6 percent / hydroxylamine hydrochloride / ethanol / 20 h / 60 °C

2: 46.2 percent / tetrahydrofuran / 12 h / Heating

With hydroxylamine hydrochloride; In tetrahydrofuran; ethanol;
DOI:10.1002/ardp.200400867