(2S,4S)-1-allyloxycarbonyl-2-(N-hydroxyacetamidine)carbamoyl-4-tritylthiopyrrolidine

Base Information

Chemical Name:(2S,4S)-1-allyloxycarbonyl-2-(N-hydroxyacetamidine)carbamoyl-4-tritylthiopyrrolidine
CAS No.:786720-37-4
Molecular Formula:C₃₀H₃₂N₄O₄S
Molecular Weight:544.674
Hs Code.:

Synonyms:(2S,4S)-1-allyloxycarbonyl-2-(N-hydroxyacetamidine)carbamoyl-4-tritylthiopyrrolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,4S)-1-allyloxycarbonyl-2-(N-hydroxyacetamidine)carbamoyl-4-tritylthiopyrrolidine

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Technology Process of (2S,4S)-1-allyloxycarbonyl-2-(N-hydroxyacetamidine)carbamoyl-4-tritylthiopyrrolidine

There total 1 articles about (2S,4S)-1-allyloxycarbonyl-2-(N-hydroxyacetamidine)carbamoyl-4-tritylthiopyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.6%

: 786720-32-9
(2S,4S)-1-allyloxycarbonyl-2-(N-cyanomethyl)carbamoyl-4-tritylthiopyrrolidine

: 786720-37-4
(2S,4S)-1-allyloxycarbonyl-2-(N-hydroxyacetamidine)carbamoyl-4-tritylthiopyrrolidine

Guidance literature:: With hydroxylamine hydrochloride; In ethanol; at 60 ℃; for 20h;
DOI:10.1002/ardp.200400867

Reference yield: 46.2%

: 4755-77-5
Ethyl oxalyl chloride

: 786720-37-4
(2S,4S)-1-allyloxycarbonyl-2-(N-hydroxyacetamidine)carbamoyl-4-tritylthiopyrrolidine

: 786720-38-5
(2S,4S)-1-allyloxycarbonyl-2-[N-(5'-ethoxycarbonyl-1',2',4'-oxadiazol-3'-yl)methyl]carbamoyl-4-tritylthiopyrrolidine

Guidance literature:: In tetrahydrofuran; for 12h; Heating;
DOI:10.1002/ardp.200400867

Reference yield:

: 786720-37-4
(2S,4S)-1-allyloxycarbonyl-2-(N-hydroxyacetamidine)carbamoyl-4-tritylthiopyrrolidine

: 786720-39-6
(2S,4S)-1-allyloxycarbonyl-2-[N-(5'-carbamoyl-1',2',4'-oxadiazol-3'-yl)methyl]carbamoyl-4-tritylthiopyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 46.2 percent / tetrahydrofuran / 12 h / Heating

2: 77.9 percent / NH₄OH / ethanol / 3 h / 60 °C

With ammonium hydroxide; In tetrahydrofuran; ethanol;
DOI:10.1002/ardp.200400867