2-formyl-5-((E)-2-phenylethen-1-yl)pyrrole

Base Information

Chemical Name:2-formyl-5-((E)-2-phenylethen-1-yl)pyrrole
CAS No.:147962-52-5
Molecular Formula:C₁₃H₁₁NO
Molecular Weight:197.236
Hs Code.:

Synonyms:2-formyl-5-((E)-2-phenylethen-1-yl)pyrrole

Suppliers and Price of 2-formyl-5-((E)-2-phenylethen-1-yl)pyrrole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of 2-formyl-5-((E)-2-phenylethen-1-yl)pyrrole

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

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Technology Process of 2-formyl-5-((E)-2-phenylethen-1-yl)pyrrole

There total 2 articles about 2-formyl-5-((E)-2-phenylethen-1-yl)pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 35563-07-6
2-((E)-2-phenylethen-1-yl)pyrrole

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 147962-52-5
2-formyl-5-((E)-2-phenylethen-1-yl)pyrrole

Guidance literature:: 2-((E)-2-phenylethen-1-yl)pyrrole; N,N-dimethyl-formamide; With trichlorophosphate; at 0 - 60 ℃; for 1.5h; Inert atmosphere;

With water; potassium carbonate; at 80 ℃; for 2h; pH=8;
DOI:10.1039/d0sc04500d

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 180283-59-4
1,1-dimethylethyl 2-ethenyl-1H-pyrrole-1-carboxylate

: 147962-52-5
2-formyl-5-((E)-2-phenylethen-1-yl)pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1.1: palladium diacetate; potassium carbonate; acetylacetone / N,N-dimethyl-formamide / 3 h / 130 °C / Inert atmosphere; Sealed tube

2.1: trichlorophosphate / 1.5 h / 0 - 60 °C / Inert atmosphere

2.2: 2 h / 80 °C / pH 8

With palladium diacetate; potassium carbonate; acetylacetone; trichlorophosphate; In N,N-dimethyl-formamide; 1.1: |Heck Reaction / 2.1: |Vilsmeier-Haack Formylation / 2.2: |Vilsmeier-Haack Formylation;
DOI:10.1039/d0sc04500d

Reference yield: 96.0%

: 147962-52-5
2-formyl-5-((E)-2-phenylethen-1-yl)pyrrole

: ammonium hexafluorophosphate

: cis-bis-(2,2′-bipyridine) dichlororuthenium(II) dihydrate

: C₃₃H₂₆N₅ORu⁽¹⁺⁾*F₆P^(1-)

Guidance literature:: 2-formyl-5-((E)-2-phenylethen-1-yl)pyrrole; cis-bis-(2,2′-bipyridine) dichlororuthenium(II) dihydrate; With triethylamine; In ethylene glycol; at 125 ℃; for 1h; Microwave irradiation; Sealed tube;

ammonium hexafluorophosphate; In water; ethylene glycol; at 20 ℃;
DOI:10.1039/d0sc04500d