methyl 3-benzyloxycarbonyl-1-(d-menthoxyacetyl)-2-oxoimidazolidine-4(S)-carboxylate

Base Information

Chemical Name:methyl 3-benzyloxycarbonyl-1-(d-menthoxyacetyl)-2-oxoimidazolidine-4(S)-carboxylate
CAS No.:459454-23-0
Molecular Formula:C₂₅H₃₄N₂O₇
Molecular Weight:474.554
Hs Code.:

Synonyms:methyl 3-benzyloxycarbonyl-1-(d-menthoxyacetyl)-2-oxoimidazolidine-4(S)-carboxylate

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Chemical Property of methyl 3-benzyloxycarbonyl-1-(d-menthoxyacetyl)-2-oxoimidazolidine-4(S)-carboxylate

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Technology Process of methyl 3-benzyloxycarbonyl-1-(d-menthoxyacetyl)-2-oxoimidazolidine-4(S)-carboxylate

There total 3 articles about methyl 3-benzyloxycarbonyl-1-(d-menthoxyacetyl)-2-oxoimidazolidine-4(S)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 15356-62-4
L-menthoxyacetyl chloride

: 168399-08-4
methyl 3-benzyloxycarbonyl-2-oxo-imidazolidine-4(S)-carboxylate

: 459454-23-0
methyl 3-benzyloxycarbonyl-1-(d-menthoxyacetyl)-2-oxoimidazolidine-4(S)-carboxylate

Guidance literature:: With pyridine; dmap; In dichloromethane; for 24h; Heating;
DOI:10.1023/A:1015061620557

Reference yield:

: 40248-63-3
menthoxyacetic acid

: 459454-23-0
methyl 3-benzyloxycarbonyl-1-(d-menthoxyacetyl)-2-oxoimidazolidine-4(S)-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 1,2-dichloro-ethane / 5 h / Heating

2: 65 percent / DMAP; pyridine / CH₂Cl₂ / 24 h / Heating

With pyridine; dmap; thionyl chloride; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1023/A:1015061620557

Reference yield:

: 59760-01-9,76497-31-9,46961-70-0
(S)-2-oxo-imidazolidine-1,5-dicarboxylic acid 1-benzyl ester

: 459454-23-0
methyl 3-benzyloxycarbonyl-1-(d-menthoxyacetyl)-2-oxoimidazolidine-4(S)-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 4.59 g / SOCl₂ / 15 h / 20 °C

2: 65 percent / DMAP; pyridine / CH₂Cl₂ / 24 h / Heating

With pyridine; dmap; thionyl chloride; In dichloromethane;
DOI:10.1023/A:1015061620557