glycylglycyl-L-phenylalanyl-L-leucine p-nitrobenzyl ester hydrobromide

Base Information

Chemical Name:glycylglycyl-L-phenylalanyl-L-leucine p-nitrobenzyl ester hydrobromide
CAS No.:75244-07-4
Molecular Formula:BrH*C₂₆H₃₃N₅O₇
Molecular Weight:608.489
Hs Code.:

Synonyms:glycylglycyl-L-phenylalanyl-L-leucine p-nitrobenzyl ester hydrobromide

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Chemical Property of glycylglycyl-L-phenylalanyl-L-leucine p-nitrobenzyl ester hydrobromide

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Technology Process of glycylglycyl-L-phenylalanyl-L-leucine p-nitrobenzyl ester hydrobromide

There total 12 articles about glycylglycyl-L-phenylalanyl-L-leucine p-nitrobenzyl ester hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.8%

: 75244-05-2
benzyloxycarbonylglycylglycyl-L-phenylalanyl-L-leucine p-nitrobenzyl ester

: 75244-07-4
glycylglycyl-L-phenylalanyl-L-leucine p-nitrobenzyl ester hydrobromide

Guidance literature:: With hydrogen bromide; In acetic acid; for 0.833333h; Ambient temperature;

Reference yield: 92.3%

: 75244-06-3
4-nitrobenzyl ester of N-t-butyloxycarbonylglycylglycyl-L-phenylalanyl-L-leucine

: 75244-07-4
glycylglycyl-L-phenylalanyl-L-leucine p-nitrobenzyl ester hydrobromide

Guidance literature:: With hydrogen bromide; In acetic acid; for 0.833333h; Ambient temperature;

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 75244-07-4
glycylglycyl-L-phenylalanyl-L-leucine p-nitrobenzyl ester hydrobromide

Guidance literature:: Multi-step reaction with 5 steps

1: 77 percent / DCCI / tetrahydrofuran / 18 h / 5 °C

2: 58.7 percent / acetic acid / tetrahydrofuran / 24 h / Ambient temperature

3: 91.7 percent / HCl / dioxane / 0.5 h / Ambient temperature

4: 71.2 percent / acetic acid / tetrahydrofuran / 48 h / Ambient temperature

5: 92.3 percent / HBr / acetic acid / 0.83 h / Ambient temperature

With hydrogenchloride; hydrogen bromide; acetic acid; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; acetic acid;