benzyloxycarbonylglycylglycyl-L-phenylalanyl-L-leucine p-nitrobenzyl ester

Base Information

Chemical Name:benzyloxycarbonylglycylglycyl-L-phenylalanyl-L-leucine p-nitrobenzyl ester
CAS No.:75244-05-2
Molecular Formula:C₃₄H₃₉N₅O₉
Molecular Weight:661.712
Hs Code.:

Synonyms:benzyloxycarbonylglycylglycyl-L-phenylalanyl-L-leucine p-nitrobenzyl ester

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Chemical Property of benzyloxycarbonylglycylglycyl-L-phenylalanyl-L-leucine p-nitrobenzyl ester

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Technology Process of benzyloxycarbonylglycylglycyl-L-phenylalanyl-L-leucine p-nitrobenzyl ester

There total 7 articles about benzyloxycarbonylglycylglycyl-L-phenylalanyl-L-leucine p-nitrobenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.7%

: 72172-28-2
3-O--hydroxy-2-phenylindenone

: 75244-04-1
glycyl-L-phenylalanyl-L-leucine p-nitrobenzyl ester hydrobromide

: 75244-05-2
benzyloxycarbonylglycylglycyl-L-phenylalanyl-L-leucine p-nitrobenzyl ester

Guidance literature:: With acetic acid; In tetrahydrofuran; for 48h; Ambient temperature;

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 75244-05-2
benzyloxycarbonylglycylglycyl-L-phenylalanyl-L-leucine p-nitrobenzyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 64 percent / DCCI / tetrahydrofuran / 18 h / 5 °C

2: 70.4 percent / acetic acid / tetrahydrofuran / 48 h / Ambient temperature

3: 90.8 percent / HBr / acetic acid / 0.83 h / Ambient temperature

4: 75 percent / acetic acid / tetrahydrofuran / 48 h / Ambient temperature

5: 95.3 percent / HBr / acetic acid / 0.83 h / Ambient temperature

6: 73.7 percent / acetic acid / tetrahydrofuran / 48 h / Ambient temperature

With hydrogen bromide; acetic acid; dicyclohexyl-carbodiimide; In tetrahydrofuran; acetic acid;

Reference yield:

: 33477-29-1
benzyloxycarbonyl-L-phenylalanyl-L-leucine p-nitrobenzyl ester

: 75244-05-2
benzyloxycarbonylglycylglycyl-L-phenylalanyl-L-leucine p-nitrobenzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 90.8 percent / HBr / acetic acid / 0.83 h / Ambient temperature

2: 75 percent / acetic acid / tetrahydrofuran / 48 h / Ambient temperature

3: 95.3 percent / HBr / acetic acid / 0.83 h / Ambient temperature

4: 73.7 percent / acetic acid / tetrahydrofuran / 48 h / Ambient temperature

With hydrogen bromide; acetic acid; In tetrahydrofuran; acetic acid;