Methyl-2-<2-(4-chlorphenyl)hydrazono>-2-<3,5-bis(trifluormethyl)phenylamino>acetat

Base Information

Chemical Name:Methyl-2-<2-(4-chlorphenyl)hydrazono>-2-<3,5-bis(trifluormethyl)phenylamino>acetat
CAS No.:76032-07-0
Molecular Formula:C₁₇H₁₂ClF₆N₃O₂
Molecular Weight:439.745
Hs Code.:

Synonyms:Methyl-2-<2-(4-chlorphenyl)hydrazono>-2-<3,5-bis(trifluormethyl)phenylamino>acetat

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl-2-<2-(4-chlorphenyl)hydrazono>-2-<3,5-bis(trifluormethyl)phenylamino>acetat

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Technology Process of Methyl-2-<2-(4-chlorphenyl)hydrazono>-2-<3,5-bis(trifluormethyl)phenylamino>acetat

There total 2 articles about Methyl-2-<2-(4-chlorphenyl)hydrazono>-2-<3,5-bis(trifluormethyl)phenylamino>acetat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 62465-90-1
methyl (N-(4-chlorophenyl)hydrazono)chloroacetate

: 328-74-5
3,5-Bis-(trifluoromethyl)aniline

: 76032-07-0
Methyl-2-<2-(4-chlorphenyl)hydrazono>-2-<3,5-bis(trifluormethyl)phenylamino>acetat

Guidance literature:: With triethylamine; In toluene; 1) 70 deg C, 30 min, 2) room temperature, 5 h;

Reference yield:

: 106-47-8
4-chloro-aniline

: 76032-07-0
Methyl-2-<2-(4-chlorphenyl)hydrazono>-2-<3,5-bis(trifluormethyl)phenylamino>acetat

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / 1) conc. HCl, NaNO₂, 2) NaOAc / H₂O / 1) 8 deg C, 2) MeOH, 6 deg C (33 percent NaOH, pH= 4.5)

2: 68 percent / Et₃N / toluene / 1) 70 deg C, 30 min, 2) room temperature, 5 h

With hydrogenchloride; sodium acetate; triethylamine; sodium nitrite; In water; toluene;