(R)-5-((5-((tert-butyldiphenylsilyl)oxy)-3-methylpentyl)thio)-1-phenyl-1H-tetrazole

Base Information

Chemical Name:(R)-5-((5-((tert-butyldiphenylsilyl)oxy)-3-methylpentyl)thio)-1-phenyl-1H-tetrazole
CAS No.:1313511-78-2
Molecular Formula:C₂₉H₃₆N₄OSSi
Molecular Weight:516.783
Hs Code.:

Synonyms:(R)-5-((5-((tert-butyldiphenylsilyl)oxy)-3-methylpentyl)thio)-1-phenyl-1H-tetrazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-5-((5-((tert-butyldiphenylsilyl)oxy)-3-methylpentyl)thio)-1-phenyl-1H-tetrazole

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Technology Process of (R)-5-((5-((tert-butyldiphenylsilyl)oxy)-3-methylpentyl)thio)-1-phenyl-1H-tetrazole

There total 1 articles about (R)-5-((5-((tert-butyldiphenylsilyl)oxy)-3-methylpentyl)thio)-1-phenyl-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1046471-35-5
(S)-5-(tert-butyldiphenylsilyloxy)-3-methylpentan-1-ol

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 1313511-78-2
(R)-5-((5-((tert-butyldiphenylsilyl)oxy)-3-methylpentyl)thio)-1-phenyl-1H-tetrazole

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1039/c0ob01253j

Reference yield: 87.0%

: 1313511-78-2
(R)-5-((5-((tert-butyldiphenylsilyl)oxy)-3-methylpentyl)thio)-1-phenyl-1H-tetrazole

: 1313511-71-5
(R)-5-((5-((tert-butyldiphenylsilyl)oxy)-3-methylpentyl)sulfonyl)-1-phenyl-1H-tetrazole

Guidance literature:: With ammonium molybdate(VI) tetrahydrate; dihydrogen peroxide; In ethanol; water; at 0 ℃;
DOI:10.1039/c0ob01253j

Reference yield:

: 1313511-78-2
(R)-5-((5-((tert-butyldiphenylsilyl)oxy)-3-methylpentyl)thio)-1-phenyl-1H-tetrazole

: 1199807-70-9
((4S,5S)-5-((S,E)-6-((tert-butyldiphenylsilyl)oxy)-4-methylhex-1-en-1-yl)-2,2-dimethyl-1,3-dioxolan-4-yl)methanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonium molybdate(VI) tetrahydrate; dihydrogen peroxide / ethanol; water / 0 °C

2.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C

2.2: 6.25 h / -78 °C

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 20 °C

With ammonium molybdate(VI) tetrahydrate; dihydrogen peroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium hexamethyldisilazane; In tetrahydrofuran; ethanol; dichloromethane; water; 2.1: Julia-Kocienski olefination / 2.2: Julia-Kocienski olefination;
DOI:10.1039/c0ob01253j