Technology Process of C35H35BN2S2
There total 4 articles about C35H35BN2S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
pyrrole; C27H27BOS2;
at 20 ℃;
for 0.5h;
Inert atmosphere;
With
boron trifluoride diethyl etherate;
at 20 ℃;
for 6h;
Inert atmosphere;
DOI:10.1039/c3cc42979b
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran / 1.5 h / -78 °C / Inert atmosphere
1.2: -78 - 20 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran / 1.5 h / -78 °C / Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere
3.1: 0.5 h / 20 °C / Inert atmosphere
3.2: 6 h / 20 °C / Inert atmosphere
With
n-butyllithium;
In
tetrahydrofuran;
DOI:10.1039/c3cc42979b
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran / 1.5 h / -78 °C / Inert atmosphere
1.2: -78 - 20 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran / 1.5 h / -78 °C / Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere
3.1: 0.5 h / 20 °C / Inert atmosphere
3.2: 6 h / 20 °C / Inert atmosphere
With
n-butyllithium;
In
tetrahydrofuran;
DOI:10.1039/c3cc42979b