2-amino-3-hydroxy-5-isobutylbenzonitrile

Base Information

Chemical Name:2-amino-3-hydroxy-5-isobutylbenzonitrile
CAS No.:1093965-94-6
Molecular Formula:C₁₁H₁₄N₂O
Molecular Weight:190.245
Hs Code.:

Synonyms:2-amino-3-hydroxy-5-isobutylbenzonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-amino-3-hydroxy-5-isobutylbenzonitrile

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Technology Process of 2-amino-3-hydroxy-5-isobutylbenzonitrile

There total 1 articles about 2-amino-3-hydroxy-5-isobutylbenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 176718-54-0
2-amino-3-methoxy-5-bromobenzonitrile

: 1093965-94-6
2-amino-3-hydroxy-5-isobutylbenzonitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / tetrahydrofuran / 2 h / 20 °C

2.1: boron tribromide / dichloromethane / 20 °C / Cooling with ice

2.2: Cooling with ice

With boron tribromide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; dichloromethane;

Reference yield: 100.0%

: 1093965-94-6
2-amino-3-hydroxy-5-isobutylbenzonitrile

: 100-39-0
benzyl bromide

: 1093965-95-7
2-amino-3-(benzyloxy)-5-isobutylbenzonitrile

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃;

Reference yield: 66.0%

: 5402-55-1
2-thiophenethanol

: 1093965-94-6
2-amino-3-hydroxy-5-isobutylbenzonitrile

: 1093966-19-8
2-amino-5-isobutyl-3-[2-(3-thienyl)ethoxy]benzonitrile

Guidance literature:: 2-thiophenethanol; With methanesulfonyl chloride; triethylamine; In ethyl acetate; for 1h; Cooling with ice;

2-amino-3-hydroxy-5-isobutylbenzonitrile; With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 4h;