diethyl 2-(benzoyloxy)-2-isopropylmalonate

Base Information Edit

Chemical Name:diethyl 2-(benzoyloxy)-2-isopropylmalonate
CAS No.:60807-00-3
Molecular Formula:C₁₇H₂₂O₆
Molecular Weight:322.358
Hs Code.:
Mol file:60807-00-3.mol

Synonyms:diethyl 2-(benzoyloxy)-2-isopropylmalonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl 2-(benzoyloxy)-2-isopropylmalonate Edit

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Technology Process of diethyl 2-(benzoyloxy)-2-isopropylmalonate

There total 1 articles about diethyl 2-(benzoyloxy)-2-isopropylmalonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 759-36-4
diethyl isopropylmalonate

: 94-36-0
dibenzoyl peroxide

: 60807-00-3
diethyl 2-(benzoyloxy)-2-isopropylmalonate

Guidance literature:: Multistep reaction; (i) NaH, benzene, (ii) /BRN= 984320/;

Reference yield:

: 60807-00-3
diethyl 2-(benzoyloxy)-2-isopropylmalonate

: 24124-03-6
isopropylbenzyloxymalonic acid diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium ethanolate / 0.13 h / 35 - 40 °C

2: sodium hydride / mineral oil; N,N-dimethyl-d₆-formamide / 2 h / 70 - 75 °C / Cooling with ice

With sodium ethanolate; sodium hydride; In N,N-dimethyl-d₆-formamide; mineral oil;
DOI:10.1080/09168451.2018.1554426