3-(O-tert-butyldimethylsilyl)-1,2-O-isopropylidene-5-O-(p-tolylsulfonyl)-α-D-xylofuranose

Base Information

Chemical Name:3-(O-tert-butyldimethylsilyl)-1,2-O-isopropylidene-5-O-(p-tolylsulfonyl)-α-D-xylofuranose
CAS No.:92413-83-7
Molecular Formula:C₂₁H₃₄O₇SSi
Molecular Weight:458.648
Hs Code.:

Synonyms:3-(O-tert-butyldimethylsilyl)-1,2-O-isopropylidene-5-O-(p-tolylsulfonyl)-α-D-xylofuranose

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Chemical Property of 3-(O-tert-butyldimethylsilyl)-1,2-O-isopropylidene-5-O-(p-tolylsulfonyl)-α-D-xylofuranose

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Technology Process of 3-(O-tert-butyldimethylsilyl)-1,2-O-isopropylidene-5-O-(p-tolylsulfonyl)-α-D-xylofuranose

There total 1 articles about 3-(O-tert-butyldimethylsilyl)-1,2-O-isopropylidene-5-O-(p-tolylsulfonyl)-α-D-xylofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 6893-65-8,20513-95-5,20513-96-6,34981-06-1,40429-51-4,110349-61-6
1,2-di-O-isopropylidene-5-O-tosyl-D-xylofuranose

: 92413-83-7
3-(O-tert-butyldimethylsilyl)-1,2-O-isopropylidene-5-O-(p-tolylsulfonyl)-α-D-xylofuranose

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; for 17h; Ambient temperature;

Reference yield: 61.0%

: 92413-83-7
3-(O-tert-butyldimethylsilyl)-1,2-O-isopropylidene-5-O-(p-tolylsulfonyl)-α-D-xylofuranose

: 108-98-5
thiophenol

: 157555-90-3
3-(O-tert-butyldimethylsilyl)-1,2-O-isopropylidene-5-S-phenyl-5-thio-α-D-xylofuranose

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In benzene; at 50 ℃; for 16h;

Reference yield:

: 92413-83-7
3-(O-tert-butyldimethylsilyl)-1,2-O-isopropylidene-5-O-(p-tolylsulfonyl)-α-D-xylofuranose

: 124502-76-7
3-(O-tert-butyldimethylsilyl)-5-chloro-1,2-O-isopropylidene-5-S-phenyl-5-thio-α-D-xylofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / DBU / benzene / 16 h / 50 °C

2: 99 percent / CCl₄, NCS / 12 h / Ambient temperature

With tetrachloromethane; N-chloro-succinimide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In benzene;