(1S,2R,4S)-2-(2-methyl-4-(dibenzylamino)cyclopentyl)-dimethylsulfoxonium-2-oxo-ethylide

Base Information

Chemical Name:(1S,2R,4S)-2-(2-methyl-4-(dibenzylamino)cyclopentyl)-dimethylsulfoxonium-2-oxo-ethylide
CAS No.:1310731-25-9
Molecular Formula:C₂₄H₃₁NO₂S
Molecular Weight:397.582
Hs Code.:

Synonyms:(1S,2R,4S)-2-(2-methyl-4-(dibenzylamino)cyclopentyl)-dimethylsulfoxonium-2-oxo-ethylide

Suppliers and Price of (1S,2R,4S)-2-(2-methyl-4-(dibenzylamino)cyclopentyl)-dimethylsulfoxonium-2-oxo-ethylide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1S,2R,4S)-2-(2-methyl-4-(dibenzylamino)cyclopentyl)-dimethylsulfoxonium-2-oxo-ethylide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1S,2R,4S)-2-(2-methyl-4-(dibenzylamino)cyclopentyl)-dimethylsulfoxonium-2-oxo-ethylide

There total 1 articles about (1S,2R,4S)-2-(2-methyl-4-(dibenzylamino)cyclopentyl)-dimethylsulfoxonium-2-oxo-ethylide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1310729-88-4
(1S,2R,4S)-4-(dibenzylamino)-2-methylcyclopentanecarboxylic acid

: 70775-39-2,5367-24-8
dimethylsulfoxonium methylide

: 1310731-25-9
(1S,2R,4S)-2-(2-methyl-4-(dibenzylamino)cyclopentyl)-dimethylsulfoxonium-2-oxo-ethylide

Guidance literature:: (1S,2R,4S)-4-(dibenzylamino)-2-methylcyclopentanecarboxylic acid; With triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; for 4h;

dimethylsulfoxonium methylide; In tetrahydrofuran; at -5 - 5 ℃; for 11h; Inert atmosphere;

Reference yield: 56.0%

: 1201187-46-3
2-amino-5-(p-toluenesulfonyl)-5H-pyrrolo[2,3-b]pyrazine

: 1310731-25-9
(1S,2R,4S)-2-(2-methyl-4-(dibenzylamino)cyclopentyl)-dimethylsulfoxonium-2-oxo-ethylide

: 1310731-26-0
1-((1S,2R,4S)-4-(dibenzylamino)-2-methylcyclopentyl)-2-(5-tosyl-5H-pyrrolo[2,3-b]pyrazin-2-ylamino)ethanone

Guidance literature:: With bis(1,5-cyclooctadiene)diiridium(I) dichloride; In chloroform; at 70 ℃; for 68h; Inert atmosphere;

Reference yield:

: 1310731-25-9
(1S,2R,4S)-2-(2-methyl-4-(dibenzylamino)cyclopentyl)-dimethylsulfoxonium-2-oxo-ethylide

: 1310731-27-1
(1S,3S,4R)-N,N-dibenzyl-3-(3H-imidazo[1,2-a]pyrrolo[2,3-e]pyrazin-8-yl)-4-methylcyclopentanamine

Guidance literature:: Multi-step reaction with 3 steps

1: bis(1,5-cyclooctadiene)diiridium(I) dichloride / chloroform / 68 h / 70 °C / Inert atmosphere

2: trifluoroacetic anhydride; trifluoroacetic acid / acetonitrile / 42 h / 40 °C / Cooling with ice

3: sodium hydroxide / tetrahydrofuran; water / 16 h / 60 °C

With bis(1,5-cyclooctadiene)diiridium(I) dichloride; trifluoroacetic acid; trifluoroacetic anhydride; sodium hydroxide; In tetrahydrofuran; chloroform; water; acetonitrile;