Technology Process of 3,6-Dioxo-1,1,1,8,8,8-hexaphenyl-2,7-dioxa-1,8-distannaoctane
There total 1 articles about 3,6-Dioxo-1,1,1,8,8,8-hexaphenyl-2,7-dioxa-1,8-distannaoctane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
acetone;
byproducts: H2O; refluxing 2:1 mixt. of (C6H5)3SnOH and acid in acetone for 2 h over molecular sieves;; azeotropical removal of H2O; recrystn. from acetone; elem. anal.;;
DOI:10.1016/0022-328X(92)83438-N