benzyl 7-(4-cyanophenylcarbamoyl)-2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoate

Base Information

Chemical Name:benzyl 7-(4-cyanophenylcarbamoyl)-2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoate
CAS No.:1308677-07-7
Molecular Formula:C₂₂H₁₂F₁₂N₂O₃
Molecular Weight:580.33
Hs Code.:

Synonyms:benzyl 7-(4-cyanophenylcarbamoyl)-2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 7-(4-cyanophenylcarbamoyl)-2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoate

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Technology Process of benzyl 7-(4-cyanophenylcarbamoyl)-2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoate

There total 2 articles about benzyl 7-(4-cyanophenylcarbamoyl)-2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 1355356-58-9
benzyl 7-chlorocarbonyl-2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoate

: 873-74-5
4-Aminobenzonitrile

: 1308677-07-7
benzyl 7-(4-cyanophenylcarbamoyl)-2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 5h; Inert atmosphere; Cooling with ice;
DOI:10.1016/j.bmc.2011.11.041

Reference yield:

: 678-45-5
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid

: 1308677-07-7
benzyl 7-(4-cyanophenylcarbamoyl)-2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoate

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride; N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux

2: 2 h / 100 °C / Inert atmosphere; Cooling with ice

3: triethylamine / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Cooling with ice

With thionyl chloride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran;
DOI:10.1016/j.bmc.2011.11.041