2-(p-cyanophenyl)-4-nitropentane

Base Information

• Chemical Name: 2-(p-cyanophenyl)-4-nitropentane
• CAS No.: 123871-56-7
• Molecular Formula: C₁₂H₁₄N₂O₂
• Molecular Weight: 218.255
• Mol file: 123871-56-7.mol

Synonyms:2-(p-cyanophenyl)-4-nitropentane

Chemical Property of 2-(p-cyanophenyl)-4-nitropentane

Chemical Property:

Purity/Quality:

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Technology Process of 2-(p-cyanophenyl)-4-nitropentane

There total 3 articles about 2-(p-cyanophenyl)-4-nitropentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

p-cyano-α-chlorocumene (72206-85-0) + lithium 1-nitroethan-1-ide (28735-55-9) → p-Cyanocumen (13816-33-6) + 2-(p-cyanophenyl)-2-methyl-3-nitrobutane (65253-36-3) + 4-(2-hydroxypropan-2-yl)benzenecarbonitrile (77802-22-3) + 2-(p-cyanophenyl)-4-nitropentane (123871-56-7)

Guidance literature:

With meta-dinitrobenzene; In N,N,N,N,N,N-hexamethylphosphoric triamide; Further byproducts given; Irradiation;

DOI:10.1016/0040-4020(89)80129-2

Reference yield: 12.0%

p-cyano-α-chlorocumene (72206-85-0) + lithium 1-nitroethan-1-ide (28735-55-9) → 2-(4-cyanophenyl)propene (19956-03-7) + 2-(p-cyanophenyl)-2-methyl-3-nitrobutane (65253-36-3) + 4-(2-hydroxypropan-2-yl)benzenecarbonitrile (77802-22-3) + 2-(p-cyanophenyl)-4-nitropentane (123871-56-7)

Guidance literature:

In N,N,N,N,N,N-hexamethylphosphoric triamide; total darkness;

DOI:10.1016/0040-4020(89)80129-2

Reference yield: 2.0%

p-cyano-α-chlorocumene (72206-85-0) + lithium 1-nitroethan-1-ide (28735-55-9) → 2-(4-cyanophenyl)propene (19956-03-7) + 2-(4-nitrophenyl)propan-2-ol (22357-57-9) + 2-(p-cyanophenyl)-4-nitropentane (123871-56-7)

Guidance literature:

With N,N-di-tert-butylnitroxide; In N,N,N,N,N,N-hexamethylphosphoric triamide; Irradiation;

DOI:10.1016/0040-4020(89)80129-2

upstream raw materials:

p-cyano-α-chlorocumene

lithium 1-nitroethan-1-ide