1,1-Dipropoxyethane

Base Information

• Chemical Name: 1,1-Dipropoxyethane
• CAS No.: 105-82-8
• Molecular Formula: C8H18 O2
• Molecular Weight: 146.23
• Hs Code.: 2909199090
• European Community (EC) Number: 203-335-2
• UNII: 277L28816Q
• DSSTox Substance ID: DTXSID5059325
• Nikkaji Number: J97.282G
• Wikidata: Q27254178
• Mol file: 105-82-8.mol

Synonyms:1,1-Dipropoxyethane;105-82-8;1-(1-Propoxyethoxy)propane;Acetaldehyde dipropyl acetal;Dipropyl acetal;n-Propyl acetal;Propane, 1,1'-[ethylidenebis(oxy)]bis-;Propane,1,1'-[ethylidenebis(oxy)]bis-;Acetaldehyde, dipropyl acetal;EINECS 203-335-2;Acetaldehyde-di-n-propyl acetal;1,1'-(Ethylidenebis(oxy))bispropane;BRN 1697928;Propane, 1,1'-(ethylidenebis(oxy))bis-;UNII-277L28816Q;277L28816Q;1,1-dipropoxyethan;1,1 - dipropoxyethane;Ethane, 1,1-dipropoxy;SCHEMBL531227;1-(1-Propoxyethoxy)propane #;Acetaldehyde di-n-propyl acetal;DTXSID5059325;FEMA NO. 4688;BCP32446;MFCD00051557;AKOS006273803;LS-7915;AS-63027;FT-0621720;D93053;Q27254178

Chemical Property of 1,1-Dipropoxyethane

Chemical Property:

• Vapor Pressure: 5.84mmHg at 25°C
• Refractive Index: 1.40174 (20℃)
• Boiling Point: 147℃ (759 Torr)
• Flash Point: 30.4±18.0℃
• PSA: 18.46000
• Density: 0.841±0.06 g/cm3 (20 ºC 760 Torr)
• LogP: 2.18560
• XLogP3: 2.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 6
• Exact Mass: 146.130679813
• Heavy Atom Count: 10
• Complexity: 56.3

Purity/Quality:

99.9% ^*data from raw suppliers

ACETALDEHYDE DIPROPYL ACETAL 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCOC(C)OCCC

Technology Process of 1,1-Dipropoxyethane

There total 11 articles about 1,1-Dipropoxyethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

propan-1-ol (71-23-8) + 2-(vinyloxy)ethyl isothiocyanate (59565-09-2) → oxazolidine-2-thione (5840-81-3) + acetaldehyde dipropyl acetal (105-82-8) + acetaldehyde propyl 2-isothiocyanatoethyl acetal (120678-96-8)

Guidance literature:

With C₃F₇COOH; at 50 - 55 ℃; for 1h;

Reference yield:

propan-1-ol (71-23-8) + LACTIC ACID (849585-22-4,106989-11-1,26811-96-1,31587-11-8,26100-51-6) → acetaldehyde dipropyl acetal (105-82-8) + 1-Propyl acetate (109-60-4) + n-propyl pyruvate (20279-43-0)

Guidance literature:

With H₅[PV₂Mo₁₀O₄₀]; at 80 ℃; for 10h; under 3750.38 Torr; Concentration; Reagent/catalyst; Temperature;

Reference yield:

propan-1-ol (71-23-8) + acetaldehyde (75-07-0,9002-91-9) → acetaldehyde dipropyl acetal (105-82-8)

Guidance literature:

With calcium chloride;

upstream raw materials:

propan-1-ol

vinyl propyl ether

acetaldehyde

tripropyl orthoformate

Downstream raw materials:

1-Propyl acetate

acetic acid

propan-1-ol

ethylpropylether

Refernces

• 1、 -. "Method for producing enol ethers". . . Retrieved 2008/06/13.
• 2、 Papsheva, N. P.,Gerasimova, V. V.,Nedolya, N. A.. "NEW SYNTHESIS OF 1,3-OXAZOLIDINE-2-THIONE". . p. 2011 - 2012. Retrieved 2007/10/02.