1-(3-Bromopropoxy)-4-chlorobenzene

Base Information

• Chemical Name: 1-(3-Bromopropoxy)-4-chlorobenzene
• CAS No.: 27983-04-6
• Molecular Formula: C9H10BrClO
• Molecular Weight: 249.535
• Hs Code.: 2909309090
• Mol file: 27983-04-6.mol

Synonyms:3-Bromopropyl 4-chlorophenyl ether;

Chemical Property of 1-(3-Bromopropoxy)-4-chlorobenzene

Chemical Property:

• Vapor Pressure: 0.00167mmHg at 25°C
• Melting Point: 34.0-35 °C(Solv: ethanol (64-17-5))
• Refractive Index: 1.551
• Boiling Point: 303.5 °C at 760 mmHg
• Flash Point: 137.3 °C
• PSA: 9.23000
• Density: 1.454 g/cm³
• LogP: 3.50380

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(3-Bromopropoxy)-4-chlorobenzene

There total 8 articles about 1-(3-Bromopropoxy)-4-chlorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-chloro-phenol (106-48-9,82344-39-6) + 1,3-dibromo-propane (109-64-8) → 1-(3-bromopropoxy)-4-chlorobenzene (27983-04-6)

Guidance literature:

With potassium carbonate; In acetonitrile; Reflux; Inert atmosphere;

DOI:10.24820/ARK.5550190.P011.262

Reference yield: 89.0%

1-allyloxy-4-chlorobenzene (13997-70-1) → 1-(3-bromopropoxy)-4-chlorobenzene (27983-04-6)

Guidance literature:

With sulfuric acid; sodium bromide; dibenzoyl peroxide; In tetrachloromethane; at 60 ℃; for 3h;

Reference yield: 34.0%

2-Bromo-1-(3-bromo-propoxy)-4-chloro-benzene (76429-75-9) → 6-chlorochromane (3722-71-2) + 1-(3-bromopropoxy)-4-chlorobenzene (27983-04-6)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; hexane; at -100 ℃; for 0.5h;

DOI:10.1021/jo00320a032

upstream raw materials:

4-chloro-phenol

1,3-dibromo-propane

2-Bromo-1-(3-bromo-propoxy)-4-chloro-benzene

2-bromo-4-chlorophenol

Downstream raw materials:

1-[3-(4-chloro-phenoxy)-propyl]-piperidine

1,3-bis-(4-chloro-phenoxy)-propane

N-[3-(4-chlorophenoxy)propyl]-N-methyl-amine

1-{4-[3-(4-Chloro-phenoxy)-propoxy]-2-hydroxy-phenyl}-ethanone

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