methanesulfonic acid 2-{2-[2-(4-{2-[2-(2-methanesulfonyloxyethoxy)ethoxy]ethoxy}phenoxy)ethoxy]ethoxy}ethyl ester

Base Information

• Chemical Name: methanesulfonic acid 2-{2-[2-(4-{2-[2-(2-methanesulfonyloxyethoxy)ethoxy]ethoxy}phenoxy)ethoxy]ethoxy}ethyl ester
• CAS No.: 882979-81-9
• Molecular Formula: C₂₀H₃₄O₁₂S₂
• Molecular Weight: 530.615

Synonyms:methanesulfonic acid 2-{2-[2-(4-{2-[2-(2-methanesulfonyloxyethoxy)ethoxy]ethoxy}phenoxy)ethoxy]ethoxy}ethyl ester

Chemical Property of methanesulfonic acid 2-{2-[2-(4-{2-[2-(2-methanesulfonyloxyethoxy)ethoxy]ethoxy}phenoxy)ethoxy]ethoxy}ethyl ester

Chemical Property:

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Technology Process of methanesulfonic acid 2-{2-[2-(4-{2-[2-(2-methanesulfonyloxyethoxy)ethoxy]ethoxy}phenoxy)ethoxy]ethoxy}ethyl ester

There total 3 articles about methanesulfonic acid 2-{2-[2-(4-{2-[2-(2-methanesulfonyloxyethoxy)ethoxy]ethoxy}phenoxy)ethoxy]ethoxy}ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1,4-bis-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)benzene (134881-72-4) + methanesulfonyl chloride (124-63-0) → methanesulfonic acid 2-{2-[2-(4-{2-[2-(2-methanesulfonyloxyethoxy)ethoxy]ethoxy}phenoxy)ethoxy]ethoxy}ethyl ester (882979-81-9)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 1.16667h;

DOI:10.1021/ja069047w

Reference yield:

hydroquinone (123-31-9,8027-02-9) → methanesulfonic acid 2-{2-[2-(4-{2-[2-(2-methanesulfonyloxyethoxy)ethoxy]ethoxy}phenoxy)ethoxy]ethoxy}ethyl ester (882979-81-9)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate; lithium bromide / N,N-dimethyl-formamide / 72 h / 80 °C / Inert atmosphere

2: triethylamine / tetrahydrofuran / 5 h / 0 - 25 °C / Inert atmosphere

With potassium carbonate; triethylamine; lithium bromide; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1021/jacs.7b06710

Reference yield:

2-[2-(chloroethoxy)ethoxy]ethanol (5197-62-6) → methanesulfonic acid 2-{2-[2-(4-{2-[2-(2-methanesulfonyloxyethoxy)ethoxy]ethoxy}phenoxy)ethoxy]ethoxy}ethyl ester (882979-81-9)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate; lithium bromide / N,N-dimethyl-formamide / 72 h / 80 °C / Inert atmosphere

2: triethylamine / tetrahydrofuran / 5 h / 0 - 25 °C / Inert atmosphere

With potassium carbonate; triethylamine; lithium bromide; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1021/jacs.7b06710

upstream raw materials:

1,4-bis-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)benzene

methanesulfonyl chloride

hydroquinone

2-[2-(chloroethoxy)ethoxy]ethanol

Downstream raw materials:

1,4-bis-{2-[-(2-iodoethoxy)ethoxy]ethoxy}benzene

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