C₃₉H₅₃O₄SiN

Base Information

Chemical Name:C₃₉H₅₃O₄SiN
CAS No.:943898-00-8
Molecular Formula:C₃₉H₅₃NO₄Si
Molecular Weight:627.94
Hs Code.:

C<sub>39</sub>H<sub>53</sub>O<sub>4</sub>SiN

Synonyms:C₃₉H₅₃O₄SiN

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Chemical Property of C₃₉H₅₃O₄SiN

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Technology Process of C₃₉H₅₃O₄SiN

There total 6 articles about C₃₉H₅₃O₄SiN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 943897-99-2
C₃₈H₅₁O₄SiN

: 74-88-4
methyl iodide

: 943898-00-8
C₃₉H₅₃O₄SiN

Guidance literature:: C₃₈H₅₁O₄SiN; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.5h;

methyl iodide; In tetrahydrofuran; at -78 ℃; for 5h; Further stages.;
DOI:10.1021/ol070517g

Reference yield:

: 633323-32-7
C₂₉H₄₄SiO₃

: 943898-00-8
C₃₉H₅₃O₄SiN

Guidance literature:: Multi-step reaction with 4 steps

1.1: 90 percent / lithium hydroxide monohydrate / tetrahydrofuran; methanol; H₂O / 5 h / 20 °C

2.1: oxalyl chloride / benzene; dimethylformamide / 4 h / 20 °C

3.1: 92 percent / butyllithium / tetrahydrofuran; hexane / -78 °C

4.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran / 0.5 h / -78 °C

4.2: 78 percent / tetrahydrofuran / 5 h / -78 °C

With lithium hydroxide; n-butyllithium; oxalyl dichloride; sodium hexamethyldisilazane; In tetrahydrofuran; methanol; hexane; water; N,N-dimethyl-formamide; benzene;
DOI:10.1021/ol070517g

Reference yield:

: C₂₈H₄₁SiO₂Cl

: 943898-00-8
C₃₉H₅₃O₄SiN

Guidance literature:: Multi-step reaction with 2 steps

1.1: 92 percent / butyllithium / tetrahydrofuran; hexane / -78 °C

2.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran / 0.5 h / -78 °C

2.2: 78 percent / tetrahydrofuran / 5 h / -78 °C

With n-butyllithium; sodium hexamethyldisilazane; In tetrahydrofuran; hexane;
DOI:10.1021/ol070517g