(2R,3S,4R,5R,6S)-5-acetamido-2-methyl-4-(naphthalen-2-ylmethoxy)-6-(p-tolylthio)tetrahydro-2H-pyran-3-yl acetate

Base Information

Chemical Name:(2R,3S,4R,5R,6S)-5-acetamido-2-methyl-4-(naphthalen-2-ylmethoxy)-6-(p-tolylthio)tetrahydro-2H-pyran-3-yl acetate
CAS No.:1395097-59-2
Molecular Formula:C₂₈H₃₁NO₅S
Molecular Weight:493.624
Hs Code.:

Synonyms:(2R,3S,4R,5R,6S)-5-acetamido-2-methyl-4-(naphthalen-2-ylmethoxy)-6-(p-tolylthio)tetrahydro-2H-pyran-3-yl acetate

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Chemical Property of (2R,3S,4R,5R,6S)-5-acetamido-2-methyl-4-(naphthalen-2-ylmethoxy)-6-(p-tolylthio)tetrahydro-2H-pyran-3-yl acetate

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Technology Process of (2R,3S,4R,5R,6S)-5-acetamido-2-methyl-4-(naphthalen-2-ylmethoxy)-6-(p-tolylthio)tetrahydro-2H-pyran-3-yl acetate

There total 1 articles about (2R,3S,4R,5R,6S)-5-acetamido-2-methyl-4-(naphthalen-2-ylmethoxy)-6-(p-tolylthio)tetrahydro-2H-pyran-3-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: (3R,4R,5S,6R)3-acetamido-6-methyl-4-(naphthalen-2-ylmethoxy)tetrahydro-2H-pyran-2,5-diyl diacetate

: 106-45-6
para-thiocresol

: 1395097-59-2
(2R,3S,4R,5R,6S)-5-acetamido-2-methyl-4-(naphthalen-2-ylmethoxy)-6-(p-tolylthio)tetrahydro-2H-pyran-3-yl acetate

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1021/ol3023227

Reference yield: 74.0%

: 920958-49-2
benzyl-(5-hydroxy-pentyl)-carbamic acid benzyl ester

: 1395097-59-2
(2R,3S,4R,5R,6S)-5-acetamido-2-methyl-4-(naphthalen-2-ylmethoxy)-6-(p-tolylthio)tetrahydro-2H-pyran-3-yl acetate

: 1395097-61-6
(2R,3S,4R,5R,6R)-5-acetamido-6-((5-(benzyl((benzyloxy)carbonyl)amino)pentyl)oxy)-2-methyl-4-(naphthalen-2-ylmethoxy)tetrahydro-2H-pyran-3-yl acetate

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In diethyl ether; dichloromethane; at 0 - 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1021/ol3023227

Reference yield: 66.0%

: 21209-51-8
N-benzyloxycarbonyl-L-serine benzyl ester

: 1395097-59-2
(2R,3S,4R,5R,6S)-5-acetamido-2-methyl-4-(naphthalen-2-ylmethoxy)-6-(p-tolylthio)tetrahydro-2H-pyran-3-yl acetate

: 1395097-60-5
(S)-benzyl 3-(((2R,3R,4R,5S,6R)-3-acetamido-5-acetoxy-6-methyl-4-(naphthalen-2-ylmethoxy)tetrahydro-2H-pyran-2-yl)oxy)-2-(((benzyloxy)carbonyl)amino)propanoate

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at 0 - 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1021/ol3023227