3-Bromo-5-methoxy-4-(phenylmethoxy)benzenemethanol

Base Information

Chemical Name:3-Bromo-5-methoxy-4-(phenylmethoxy)benzenemethanol
CAS No.:73304-09-3
Molecular Formula:C₁₅H₁₅BrO₃
Molecular Weight:323.186
Hs Code.:
DSSTox Substance ID:DTXSID701229624

Synonyms:3-Bromo-5-methoxy-4-(phenylmethoxy)benzenemethanol;DTXSID701229624;AKOS000291644;73304-09-3;(4-(Benzyloxy)-3-bromo-5-methoxyphenyl)methanol

Suppliers and Price of 3-Bromo-5-methoxy-4-(phenylmethoxy)benzenemethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Bromo-5-methoxy-4-(phenylmethoxy)benzenemethanol

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:322.02046
Heavy Atom Count:19
Complexity:256

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C(=CC(=C1)CO)Br)OCC2=CC=CC=C2

Technology Process of 3-Bromo-5-methoxy-4-(phenylmethoxy)benzenemethanol

There total 3 articles about 3-Bromo-5-methoxy-4-(phenylmethoxy)benzenemethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 2556-04-9
4-(benzyloxy)-3-bromo-5-methoxybenzaldehyde

: 73304-09-3
[4-(benzyloxy)-3-bromo-5-methoxyphenyl]methanol

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 0 - 20 ℃; for 2h;
DOI:10.1021/acs.joc.6b02647

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 73304-09-3
[4-(benzyloxy)-3-bromo-5-methoxyphenyl]methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / Br₂ / CCl₄; CHCl₃ / 5 h / 20 °C

2: ethyldiisopropylamine / CH₂Cl₂ / 72 h / 20 °C

3: 6.2 g / NaBH₄ / methanol

With sodium tetrahydroborate; bromine; N-ethyl-N,N-diisopropylamine; In methanol; tetrachloromethane; dichloromethane; chloroform;
DOI:10.1021/jm050139q