C₁₅H₂₀FN₃O₂

Base Information

Chemical Name:C₁₅H₂₀FN₃O₂
CAS No.:1198223-34-5
Molecular Formula:C₁₅H₂₀FN₃O₂
Molecular Weight:293.341
Hs Code.:

C<sub>15</sub>H<sub>20</sub>FN<sub>3</sub>O<sub>2</sub>

Synonyms:C₁₅H₂₀FN₃O₂

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Chemical Property of C₁₅H₂₀FN₃O₂

Chemical Property:

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Technology Process of C₁₅H₂₀FN₃O₂

There total 9 articles about C₁₅H₂₀FN₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₂₃FO₅S

: 1198223-34-5
C₁₅H₂₀FN₃O₂

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 75 ℃; for 15h;

Reference yield:

: 51446-31-2
4-fluoro-3-hydroxybenzoic acid

: 1198223-34-5
C₁₅H₂₀FN₃O₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: sulfuric acid / 4 h / 105 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 125 °C

3.1: water; sodium hydroxide / ethanol / 3 h / 55 °C

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.08 h / 20 °C

4.2: 13 h / 20 °C

5.1: tetrahydrofuran / 2.5 h / 0 °C

6.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 0 °C

6.2: 3 h / -78 - 20 °C

7.1: potassium osmate(VI); water; potassium carbonate; hydroquinidein 1,4-phthalazinediyl diether; potassium hexacyanoferrate(III) / tert-butyl alcohol / 5 h / 0 °C

8.1: triethylamine / dichloromethane / 0.5 h / 0 - 20 °C

9.1: sodium azide / N,N-dimethyl-formamide / 15 h / 75 °C

With potassium osmate(VI); sodium azide; sulfuric acid; water; sodium hexamethyldisilazane; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydroquinidein 1,4-phthalazinediyl diether; triethylamine; sodium hydroxide; potassium hexacyanoferrate(III); In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: 351317-28-7
ethyl 3-hydroxy-4-fluorobenzoate

: 1198223-34-5
C₁₅H₂₀FN₃O₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 125 °C

2.1: water; sodium hydroxide / ethanol / 3 h / 55 °C

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.08 h / 20 °C

3.2: 13 h / 20 °C

4.1: tetrahydrofuran / 2.5 h / 0 °C

5.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 0 °C

5.2: 3 h / -78 - 20 °C

6.1: potassium osmate(VI); water; potassium carbonate; hydroquinidein 1,4-phthalazinediyl diether; potassium hexacyanoferrate(III) / tert-butyl alcohol / 5 h / 0 °C

7.1: triethylamine / dichloromethane / 0.5 h / 0 - 20 °C

8.1: sodium azide / N,N-dimethyl-formamide / 15 h / 75 °C

With potassium osmate(VI); sodium azide; water; sodium hexamethyldisilazane; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydroquinidein 1,4-phthalazinediyl diether; triethylamine; sodium hydroxide; potassium hexacyanoferrate(III); In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;