N-(3',4'-Methylendioxyphenethyl)-2-brom-3-benzyloxy-3-methoxy-phenylacetamid

Base Information

Chemical Name:N-(3',4'-Methylendioxyphenethyl)-2-brom-3-benzyloxy-3-methoxy-phenylacetamid
CAS No.:116861-68-8
Molecular Formula:C₂₅H₂₄BrNO₅
Molecular Weight:498.373
Hs Code.:

Synonyms:N-(3',4'-Methylendioxyphenethyl)-2-brom-3-benzyloxy-3-methoxy-phenylacetamid

Suppliers and Price of N-(3',4'-Methylendioxyphenethyl)-2-brom-3-benzyloxy-3-methoxy-phenylacetamid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3',4'-Methylendioxyphenethyl)-2-brom-3-benzyloxy-3-methoxy-phenylacetamid

Chemical Property:

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Technology Process of N-(3',4'-Methylendioxyphenethyl)-2-brom-3-benzyloxy-3-methoxy-phenylacetamid

There total 4 articles about N-(3',4'-Methylendioxyphenethyl)-2-brom-3-benzyloxy-3-methoxy-phenylacetamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 38849-42-2
2-Brom-3-benzyloxy-4-methoxy-phenylessigsaeure

: 1484-85-1
3,4-methylenedioxyphenylethylamine

: 116861-68-8
N-(3',4'-Methylendioxyphenethyl)-2-brom-3-benzyloxy-3-methoxy-phenylacetamid

Guidance literature:: With sodium hydrogencarbonate; In xylene; for 16h; Heating;
DOI:10.1002/ardp.19883210308

Reference yield:

: 2973-58-2
2-bromoisovanillin

: 116861-68-8
N-(3',4'-Methylendioxyphenethyl)-2-brom-3-benzyloxy-3-methoxy-phenylacetamid

Guidance literature:: Multi-step reaction with 4 steps

2: 68 percent / SnCl₂*2H₂O, conc. HCl / acetic acid / 4 h / 100 °C

3: 87 percent / NaOH / methanol / 3 h / Heating

4: 54 percent / NaHCO₃ / xylene / 16 h / Heating

With hydrogenchloride; sodium hydroxide; sodium hydrogencarbonate; tin(ll) chloride; In methanol; acetic acid; xylene;
DOI:10.1002/ardp.19883210308

Reference yield:

: 116861-66-6
2-Brom-3-hydroxy-4-methoxy-mandelsaeurenitril

: 116861-68-8
N-(3',4'-Methylendioxyphenethyl)-2-brom-3-benzyloxy-3-methoxy-phenylacetamid

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / SnCl₂*2H₂O, conc. HCl / acetic acid / 4 h / 100 °C

2: 87 percent / NaOH / methanol / 3 h / Heating

3: 54 percent / NaHCO₃ / xylene / 16 h / Heating

With hydrogenchloride; sodium hydroxide; sodium hydrogencarbonate; tin(ll) chloride; In methanol; acetic acid; xylene;
DOI:10.1002/ardp.19883210308