methyl 2-[1-(2-{[(4-bromophenyl)sulfonyl]amino}phenylthio)cyclopropyl]-2-chloroacetate

Base Information

Chemical Name:methyl 2-[1-(2-{[(4-bromophenyl)sulfonyl]amino}phenylthio)cyclopropyl]-2-chloroacetate
CAS No.:552832-44-7
Molecular Formula:C₁₈H₁₇BrClNO₄S₂
Molecular Weight:490.826
Hs Code.:

Synonyms:methyl 2-[1-(2-{[(4-bromophenyl)sulfonyl]amino}phenylthio)cyclopropyl]-2-chloroacetate

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Chemical Property of methyl 2-[1-(2-{[(4-bromophenyl)sulfonyl]amino}phenylthio)cyclopropyl]-2-chloroacetate

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Technology Process of methyl 2-[1-(2-{[(4-bromophenyl)sulfonyl]amino}phenylthio)cyclopropyl]-2-chloroacetate

There total 3 articles about methyl 2-[1-(2-{[(4-bromophenyl)sulfonyl]amino}phenylthio)cyclopropyl]-2-chloroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 98-58-8
4-bromobenzenesulfonyl chloride

: 552832-38-9
methyl 2-[1-(2-aminophenylthio)cyclopropyl]-2-chloroacetate

: 552832-44-7
methyl 2-[1-(2-{[(4-bromophenyl)sulfonyl]amino}phenylthio)cyclopropyl]-2-chloroacetate

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 20h;
DOI:10.1002/ejoc.200390154

Reference yield:

: 82979-45-1
methyl 2-chloro-2-cyclopropylideneacetate

: 552832-44-7
methyl 2-[1-(2-{[(4-bromophenyl)sulfonyl]amino}phenylthio)cyclopropyl]-2-chloroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / Et₃N / CH₂Cl₂ / 24 h / 20 °C

2: 81 percent / pyridine / CH₂Cl₂ / 20 h / 20 °C

With pyridine; triethylamine; In dichloromethane;
DOI:10.1002/ejoc.200390154

Reference yield:

: 137-07-5
2-amino-benzenethiol

: 552832-44-7
methyl 2-[1-(2-{[(4-bromophenyl)sulfonyl]amino}phenylthio)cyclopropyl]-2-chloroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / Et₃N / CH₂Cl₂ / 24 h / 20 °C

2: 81 percent / pyridine / CH₂Cl₂ / 20 h / 20 °C

With pyridine; triethylamine; In dichloromethane;
DOI:10.1002/ejoc.200390154