C₂₃H₂₈N₂O₆

Base Information

Chemical Name:C₂₃H₂₈N₂O₆
CAS No.:431052-68-5
Molecular Formula:C₂₃H₂₈N₂O₆
Molecular Weight:428.485
Hs Code.:

C<sub>23</sub>H<sub>28</sub>N<sub>2</sub>O<sub>6</sub>

Synonyms:C₂₃H₂₈N₂O₆

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Chemical Property of C₂₃H₂₈N₂O₆

Chemical Property:

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Technology Process of C₂₃H₂₈N₂O₆

There total 12 articles about C₂₃H₂₈N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: C₂₄H₃₀N₂O₆

: 431052-68-5
C₂₃H₂₈N₂O₆

Guidance literature:: With water; sodium hydroxide; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2013.06.028

Reference yield:

: 1121-60-4
pyridine-2-carbaldehyde

: 431052-68-5
C₂₃H₂₈N₂O₆

Guidance literature:: Multi-step reaction with 7 steps

1: N,N',N'-trimethylenediamine; n-butyllithium / tetrahydrofuran; hexane; cyclohexane

2: sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene / tert-butyl alcohol; acetonitrile; water

3: caesium carbonate / N,N-dimethyl-formamide

4: 3-chloro-benzenecarboperoxoic acid / dichloromethane

5: bis-triphenylphosphine-palladium(II) chloride; copper(II) oxide / N,N-dimethyl-formamide / 110 °C

6: trifluoroacetic anhydride / N,N-dimethyl-formamide

7: sodium hydroxide; water / tetrahydrofuran

With bis-triphenylphosphine-palladium(II) chloride; sodium chlorite; n-butyllithium; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; water; caesium carbonate; N,N',N'-trimethylenediamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride; copper(II) oxide; sodium hydroxide; In tetrahydrofuran; hexane; dichloromethane; cyclohexane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2013.06.028

Reference yield:

: 431052-64-1
3-(tributylstannyl)picolinaldehyde

: 431052-68-5
C₂₃H₂₈N₂O₆

Guidance literature:: Multi-step reaction with 6 steps

1: sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene / tert-butyl alcohol; acetonitrile; water

2: caesium carbonate / N,N-dimethyl-formamide

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane

4: bis-triphenylphosphine-palladium(II) chloride; copper(II) oxide / N,N-dimethyl-formamide / 110 °C

5: trifluoroacetic anhydride / N,N-dimethyl-formamide

6: sodium hydroxide; water / tetrahydrofuran

With bis-triphenylphosphine-palladium(II) chloride; sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; water; caesium carbonate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride; copper(II) oxide; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2013.06.028