2-(<3'-(1-thio-2-(phenylphosphino)phenyl)propyl>phenylphosphino)thiobenzene

Base Information

Chemical Name:2-(<3'-(1-thio-2-(phenylphosphino)phenyl)propyl>phenylphosphino)thiobenzene
CAS No.:94904-40-2
Molecular Formula:C₂₇H₂₆P₂S₂
Molecular Weight:476.583
Hs Code.:

Synonyms:2-(<3'-(1-thio-2-(phenylphosphino)phenyl)propyl>phenylphosphino)thiobenzene

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Chemical Property of 2-(<3'-(1-thio-2-(phenylphosphino)phenyl)propyl>phenylphosphino)thiobenzene

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Technology Process of 2-(<3'-(1-thio-2-(phenylphosphino)phenyl)propyl>phenylphosphino)thiobenzene

There total 8 articles about 2-(<3'-(1-thio-2-(phenylphosphino)phenyl)propyl>phenylphosphino)thiobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65000-89-7
Ethyl-(o-nitrophenyl)-phenylphosphinat

: 94904-40-2
2-(<3'-(1-thio-2-(phenylphosphino)phenyl)propyl>phenylphosphino)thiobenzene

Guidance literature:: Multi-step reaction with 6 steps

1: Fe, NH₄Cl / H₂O / Heating

3: 76 percent

4: 96 percent / 2.64 M n-butyllithium / hexane; tetrahydrofuran / -78 °C

5: potassium hydroxide / tetrahydrofuran; aq. ethanol / 106 h / Ambient temperature

6: sodium butylthiolate / dimethylformamide / 9 h / 80 °C

With potassium hydroxide; n-butyllithium; sodium 1-buthanethiolate; iron; ammonium chloride; In tetrahydrofuran; ethanol; hexane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja00293a052

Reference yield:

: 1638-86-4
diethyl phenylphosphonite

: 94904-40-2
2-(<3'-(1-thio-2-(phenylphosphino)phenyl)propyl>phenylphosphino)thiobenzene

Guidance literature:: Multi-step reaction with 7 steps

1: 25 °C

2: Fe, NH₄Cl / H₂O / Heating

4: 76 percent

5: 96 percent / 2.64 M n-butyllithium / hexane; tetrahydrofuran / -78 °C

6: potassium hydroxide / tetrahydrofuran; aq. ethanol / 106 h / Ambient temperature

7: sodium butylthiolate / dimethylformamide / 9 h / 80 °C

With potassium hydroxide; n-butyllithium; sodium 1-buthanethiolate; iron; ammonium chloride; In tetrahydrofuran; ethanol; hexane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja00293a052

Reference yield:

: 93383-27-8
1-thio-2-(phenylphosphino)benzene

: 94904-40-2
2-(<3'-(1-thio-2-(phenylphosphino)phenyl)propyl>phenylphosphino)thiobenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent

2: 96 percent / 2.64 M n-butyllithium / hexane; tetrahydrofuran / -78 °C

3: potassium hydroxide / tetrahydrofuran; aq. ethanol / 106 h / Ambient temperature

4: sodium butylthiolate / dimethylformamide / 9 h / 80 °C

With potassium hydroxide; n-butyllithium; sodium 1-buthanethiolate; In tetrahydrofuran; ethanol; hexane; N,N-dimethyl-formamide;
DOI:10.1021/ja00293a052