4-(2-methyl-2-propen-1-yl)-3,5-diphenylisoxazole

Base Information

Chemical Name:4-(2-methyl-2-propen-1-yl)-3,5-diphenylisoxazole
CAS No.:1227782-05-9
Molecular Formula:C₁₉H₁₇NO
Molecular Weight:275.35
Hs Code.:

Synonyms:4-(2-methyl-2-propen-1-yl)-3,5-diphenylisoxazole

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Chemical Property of 4-(2-methyl-2-propen-1-yl)-3,5-diphenylisoxazole

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Technology Process of 4-(2-methyl-2-propen-1-yl)-3,5-diphenylisoxazole

There total 5 articles about 4-(2-methyl-2-propen-1-yl)-3,5-diphenylisoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 870127-38-1
(Z)-1,3-diphenylprop-2-yn-1-one O-methyl oxime

: 1458-98-6
2-methyl-3-bromo-1-propene

: 1227782-05-9
4-(2-methyl-2-propen-1-yl)-3,5-diphenylisoxazole

Guidance literature:: With tetrabutylammomium bromide; palladium diacetate; In N,N-dimethyl-formamide; at 80 ℃; for 0.5h;
DOI:10.1021/acs.joc.9b01593

Reference yield: 91.0%

: 28164-35-4
1,3-diphenylprop-2-yn-1-one oxime

: 513-42-8
3-hydroxy-2-methyl-1-propene

: 1227782-05-9
4-(2-methyl-2-propen-1-yl)-3,5-diphenylisoxazole

Guidance literature:: With 1-(carboxymethyl)-3-methylimidazolium chloride; (3-phenylallyl)(chloro)-[1,3-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene]palladium(II); oxygen; In water; at 110 ℃; for 12h; Green chemistry;
DOI:10.1039/d0gc02037k

Reference yield: 78.0%

: 1227781-87-4
(1Z)-1,3-diphenyl-2-propyn-1-one O-(2-methyl-2-propen-1-yl)oxime

: 1227782-05-9
4-(2-methyl-2-propen-1-yl)-3,5-diphenylisoxazole

Guidance literature:: With gold(III) chloride; In trans-1,2-dichloroethylene; at 20 ℃; regioselective reaction; Inert atmosphere; Reflux;
DOI:10.1021/ol100803e