Technology Process of (R)-2-(benzyloxy)-1-dodecanol
There total 9 articles about (R)-2-(benzyloxy)-1-dodecanol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
diethyl ether;
for 0.166667h;
Ambient temperature;
DOI:10.1021/jo00376a056
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 92 percent / sodium hydride / tetrahydrofuran / 10 h / Heating
2: 1.) N-chlorosuccinimide, silver nitrate, sodium bicarbonate, 2.) potassium dihydrogen phosphate, sodium chloride / 1.) acetone, water, RT, 10 min, 2.) acetone,water, RT, 30 min
3: diethyl ether
4: 97 percent / LiAlH4 / diethyl ether / 0.17 h / Ambient temperature
With
potassium dihydrogenphosphate; N-chloro-succinimide; lithium aluminium tetrahydride; sodium hydride; sodium hydrogencarbonate; silver nitrate; sodium chloride;
In
tetrahydrofuran; diethyl ether;
DOI:10.1021/jo00376a056
- Guidance literature:
-
Multi-step reaction with 5 steps
1: L-selectride, LiI / toluene / 4 h / -78 °C
2: 92 percent / sodium hydride / tetrahydrofuran / 10 h / Heating
3: 1.) N-chlorosuccinimide, silver nitrate, sodium bicarbonate, 2.) potassium dihydrogen phosphate, sodium chloride / 1.) acetone, water, RT, 10 min, 2.) acetone,water, RT, 30 min
4: diethyl ether
5: 97 percent / LiAlH4 / diethyl ether / 0.17 h / Ambient temperature
With
potassium dihydrogenphosphate; N-chloro-succinimide; lithium aluminium tetrahydride; L-Selectride; sodium hydride; sodium hydrogencarbonate; silver nitrate; sodium chloride; lithium iodide;
In
tetrahydrofuran; diethyl ether; toluene;
DOI:10.1021/jo00376a056
