Dodecanoic acid, 2-(phenylmethoxy)-, methyl ester, (R)-

Base Information

Chemical Name:Dodecanoic acid, 2-(phenylmethoxy)-, methyl ester, (R)-
CAS No.:105581-76-8
Molecular Formula:C20H32O3
Molecular Weight:320.472
Hs Code.:
Mol file:105581-76-8.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dodecanoic acid, 2-(phenylmethoxy)-, methyl ester, (R)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Dodecanoic acid, 2-(phenylmethoxy)-, methyl ester, (R)-

There total 6 articles about Dodecanoic acid, 2-(phenylmethoxy)-, methyl ester, (R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 105581-76-8
methyl (R)-2-(benzyloxy)dodecanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / sodium hydride / tetrahydrofuran / 10 h / Heating

2: 1.) N-chlorosuccinimide, silver nitrate, sodium bicarbonate, 2.) potassium dihydrogen phosphate, sodium chloride / 1.) acetone, water, RT, 10 min, 2.) acetone,water, RT, 30 min

3: diethyl ether

With potassium dihydrogenphosphate; N-chloro-succinimide; sodium hydride; sodium hydrogencarbonate; silver nitrate; sodium chloride; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo00376a056

Reference yield:

: 1-((4aR,7R,8aR)-4,4,7-Trimethyl-hexahydro-1-oxa-3-thia-naphthalen-2-yl)-undecan-1-one

: 105581-76-8
methyl (R)-2-(benzyloxy)dodecanoate

Guidance literature:: Multi-step reaction with 4 steps

1: L-selectride, LiI / toluene / 4 h / -78 °C

2: 92 percent / sodium hydride / tetrahydrofuran / 10 h / Heating

3: 1.) N-chlorosuccinimide, silver nitrate, sodium bicarbonate, 2.) potassium dihydrogen phosphate, sodium chloride / 1.) acetone, water, RT, 10 min, 2.) acetone,water, RT, 30 min

4: diethyl ether

With potassium dihydrogenphosphate; N-chloro-succinimide; L-Selectride; sodium hydride; sodium hydrogencarbonate; silver nitrate; sodium chloride; lithium iodide; In tetrahydrofuran; diethyl ether; toluene;
DOI:10.1021/jo00376a056

Reference yield:

: 1-((4aR,7R,8aR)-4,4,7-Trimethyl-hexahydro-1-oxa-3-thia-naphthalen-2-yl)-undecan-1-ol

: 105581-76-8
methyl (R)-2-(benzyloxy)dodecanoate

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / chromium trioxide, pyridine / CH₂Cl₂ / 1 h / Ambient temperature

2: L-selectride, LiI / toluene / 4 h / -78 °C

3: 92 percent / sodium hydride / tetrahydrofuran / 10 h / Heating

4: 1.) N-chlorosuccinimide, silver nitrate, sodium bicarbonate, 2.) potassium dihydrogen phosphate, sodium chloride / 1.) acetone, water, RT, 10 min, 2.) acetone,water, RT, 30 min

5: diethyl ether

With pyridine; chromium(VI) oxide; potassium dihydrogenphosphate; N-chloro-succinimide; L-Selectride; sodium hydride; sodium hydrogencarbonate; silver nitrate; sodium chloride; lithium iodide; In tetrahydrofuran; diethyl ether; dichloromethane; toluene;
DOI:10.1021/jo00376a056