Technology Process of C25H29FN4O7
There total 3 articles about C25H29FN4O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C28H35FN4O7;
With
trifluoroacetic acid;
In
dichloromethane;
methanol;
With
thionyl chloride;
at 0 - 20 ℃;
DOI:10.1071/CH13590
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 6 h / 40 °C
2.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C
3.1: trifluoroacetic acid / dichloromethane
3.2: 0 - 20 °C
With
di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; acetic acid; triphenylphosphine; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane;
2.1: |Mitsunobu Displacement;
DOI:10.1071/CH13590
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: acetic acid; palladium hydroxide, 20 wt% on carbon; hydrogen / methanol; ethyl acetate / 2.5 h / 760.05 Torr
1.2: 1 h
2.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 6 h / 40 °C
3.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C
4.1: trifluoroacetic acid / dichloromethane
4.2: 0 - 20 °C
With
di-isopropyl azodicarboxylate; palladium hydroxide, 20 wt% on carbon; tetrabutyl ammonium fluoride; hydrogen; acetic acid; triphenylphosphine; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate;
3.1: |Mitsunobu Displacement;
DOI:10.1071/CH13590
