3-(4-METHOXYPHENYL)-3-OXO-2-(2-PHENYLHYDRAZONO)PROPANAL

Base Information

• Chemical Name: 3-(4-METHOXYPHENYL)-3-OXO-2-(2-PHENYLHYDRAZONO)PROPANAL
• CAS No.: 60083-35-4
• Molecular Formula: C₁₆H₁₄N₂O₃
• Molecular Weight: 282.299
• Mol file: 60083-35-4.mol

Synonyms:3-(4-methoxy-phenyl)-3-oxo-2-phenylhydrazono-propionaldehyde

Chemical Property of 3-(4-METHOXYPHENYL)-3-OXO-2-(2-PHENYLHYDRAZONO)PROPANAL

Chemical Property:

Purity/Quality:

3-(4-METHOXYPHENYL)-3-OXO-2-(2-PHENYLHYDRAZONO)PROPANAL 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(4-METHOXYPHENYL)-3-OXO-2-(2-PHENYLHYDRAZONO)PROPANAL

There total 2 articles about 3-(4-METHOXYPHENYL)-3-OXO-2-(2-PHENYLHYDRAZONO)PROPANAL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzene diazonium chloride (100-34-5) + 3-dimethylamino-4'-methoxyacrylophenone (18096-70-3,78090-00-3) → 3-(4-Methoxy-phenyl)-3-oxo-2-(phenyl-hydrazono)-propionaldehyde (60083-35-4) + 3-(4-methoxyphenyl)-3-oxo-2-(phenylhydrazono)propanal

Guidance literature:

With sodium hydroxide; In ethanol; at 20 ℃; for 1h; Title compound not separated from byproducts;

DOI:10.1016/S0040-4020(00)01141-8

Reference yield:

benzene diazonium chloride (100-34-5) → 3-(4-methoxy-phenyl)-3-oxo-2-phenylhydrazono-propionaldehyde (60083-35-4)

Guidance literature:

Reference yield: 82.0%

3-(4-methoxy-phenyl)-3-oxo-2-phenylhydrazono-propionaldehyde (60083-35-4) → 4,8-di(4-methoxybenzoyl)-2,6-diphenyl-2,3,6,7,9-pentaazabicyclo[3.3.1]nona-3,7-diene

Guidance literature:

With ammonium acetate; triethylamine; In ethanol; at 80 ℃; for 0.0833333h; Microwave irradiation;

DOI:10.3390/molecules24061110

upstream raw materials:

benzene diazonium chloride

3-dimethylamino-4'-methoxyacrylophenone

Downstream raw materials:

1-(4-Methoxy-phenyl)-3-[(E)-4-methoxy-phenylimino]-2-(phenyl-hydrazono)-propan-1-one

1-(4-Methoxy-phenyl)-2-(phenyl-hydrazono)-3-[(E)-phenylimino]-propan-1-one

(cinnolin-3-yl)(4-methoxyphenyl)methanone

4-methoxybenzoyl cyanide

Refernces