2,2-dimethyl-propionic acid 8-(1-phenyl-1H-tetrazole-5-sulfonyl)-octyl ester

Base Information

Chemical Name:2,2-dimethyl-propionic acid 8-(1-phenyl-1H-tetrazole-5-sulfonyl)-octyl ester
CAS No.:934502-91-7
Molecular Formula:C₂₀H₃₀N₄O₄S
Molecular Weight:422.549
Hs Code.:

Synonyms:2,2-dimethyl-propionic acid 8-(1-phenyl-1H-tetrazole-5-sulfonyl)-octyl ester

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Chemical Property of 2,2-dimethyl-propionic acid 8-(1-phenyl-1H-tetrazole-5-sulfonyl)-octyl ester

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Technology Process of 2,2-dimethyl-propionic acid 8-(1-phenyl-1H-tetrazole-5-sulfonyl)-octyl ester

There total 5 articles about 2,2-dimethyl-propionic acid 8-(1-phenyl-1H-tetrazole-5-sulfonyl)-octyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 934502-91-7
2,2-dimethyl-propionic acid 8-(1-phenyl-1H-tetrazole-5-sulfonyl)-octyl ester

: 1411489-74-1
9-((1S,2R)-2-((S)-4-oxobutan-2-yl)cyclopropyl)nonyl pivalate

Guidance literature:: In dichloromethane;

Reference yield: 89.0%

: 943962-73-0
2,2-dimethyl propionic acid 8-(1-phenyl-1H-tetrazol-5-yl-sulfanyl)octyl ester

: 934502-91-7
2,2-dimethyl-propionic acid 8-(1-phenyl-1H-tetrazole-5-sulfonyl)-octyl ester

Guidance literature:: With ammonium molybdate tetrahydrate; dihydrogen peroxide; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1016/j.tet.2007.01.007

Reference yield:

: 943962-72-9
2,2-dimethyl-propionic acid 8-bromooctyl ester

: 934502-91-7
2,2-dimethyl-propionic acid 8-(1-phenyl-1H-tetrazole-5-sulfonyl)-octyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / potassium carbonate / acetone / 16 h / 20 °C

2: 89 percent / ammonium molybdate(VI) tetrahydrate; aq. hydrogen peroxide / tetrahydrofuran; various solvent(s) / 2 h / 20 °C

With ammonium molybdate tetrahydrate; dihydrogen peroxide; potassium carbonate; In tetrahydrofuran; acetone;
DOI:10.1016/j.tet.2007.01.007