2,2-dimethyl propionic acid 8-(1-phenyl-1H-tetrazol-5-yl-sulfanyl)octyl ester

Base Information

Chemical Name:2,2-dimethyl propionic acid 8-(1-phenyl-1H-tetrazol-5-yl-sulfanyl)octyl ester
CAS No.:943962-73-0
Molecular Formula:C₂₀H₃₀N₄O₂S
Molecular Weight:390.55
Hs Code.:

Synonyms:2,2-dimethyl propionic acid 8-(1-phenyl-1H-tetrazol-5-yl-sulfanyl)octyl ester

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Chemical Property of 2,2-dimethyl propionic acid 8-(1-phenyl-1H-tetrazol-5-yl-sulfanyl)octyl ester

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Technology Process of 2,2-dimethyl propionic acid 8-(1-phenyl-1H-tetrazol-5-yl-sulfanyl)octyl ester

There total 3 articles about 2,2-dimethyl propionic acid 8-(1-phenyl-1H-tetrazol-5-yl-sulfanyl)octyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 943962-72-9
2,2-dimethyl-propionic acid 8-bromooctyl ester

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 943962-73-0
2,2-dimethyl propionic acid 8-(1-phenyl-1H-tetrazol-5-yl-sulfanyl)octyl ester

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 16h;
DOI:10.1016/j.tet.2007.01.007

Reference yield:

: 50816-19-8
8-bromooctanol

: 943962-73-0
2,2-dimethyl propionic acid 8-(1-phenyl-1H-tetrazol-5-yl-sulfanyl)octyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / triethylamine; 4-dimethylaminopyridine / CH₂Cl₂ / 16 h / 20 °C

2: 90 percent / potassium carbonate / acetone / 16 h / 20 °C

With dmap; potassium carbonate; triethylamine; In dichloromethane; acetone;
DOI:10.1016/j.tet.2007.01.007

Reference yield:

: 3282-30-2
pivaloyl chloride

: 943962-73-0
2,2-dimethyl propionic acid 8-(1-phenyl-1H-tetrazol-5-yl-sulfanyl)octyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / triethylamine; 4-dimethylaminopyridine / CH₂Cl₂ / 16 h / 20 °C

2: 90 percent / potassium carbonate / acetone / 16 h / 20 °C

With dmap; potassium carbonate; triethylamine; In dichloromethane; acetone;
DOI:10.1016/j.tet.2007.01.007