9-[4-(3-tert-butoxycarbonylmethoxypropyl)-(methyl)-aminomethylbenzyl]-7,8-dihydro-2-(2-methoxyethoxy)-8-oxoadenine

Base Information

Chemical Name:9-[4-(3-tert-butoxycarbonylmethoxypropyl)-(methyl)-aminomethylbenzyl]-7,8-dihydro-2-(2-methoxyethoxy)-8-oxoadenine
CAS No.:930294-40-9
Molecular Formula:C₂₆H₃₈N₆O₆
Molecular Weight:530.624
Hs Code.:

Synonyms:9-[4-(3-tert-butoxycarbonylmethoxypropyl)-(methyl)-aminomethylbenzyl]-7,8-dihydro-2-(2-methoxyethoxy)-8-oxoadenine

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Chemical Property of 9-[4-(3-tert-butoxycarbonylmethoxypropyl)-(methyl)-aminomethylbenzyl]-7,8-dihydro-2-(2-methoxyethoxy)-8-oxoadenine

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Technology Process of 9-[4-(3-tert-butoxycarbonylmethoxypropyl)-(methyl)-aminomethylbenzyl]-7,8-dihydro-2-(2-methoxyethoxy)-8-oxoadenine

There total 1 articles about 9-[4-(3-tert-butoxycarbonylmethoxypropyl)-(methyl)-aminomethylbenzyl]-7,8-dihydro-2-(2-methoxyethoxy)-8-oxoadenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 930294-39-6
tert-butyl 2-(3-oxopropoxy)acetate

: 930294-32-9
6-amino-2-(2-methoxyethoxy)-9-(4-((methylamino)methyl)benzyl)-7,9-dihydro-8H-purin-8-one

: 930294-40-9
9-[4-(3-tert-butoxycarbonylmethoxypropyl)-(methyl)-aminomethylbenzyl]-7,8-dihydro-2-(2-methoxyethoxy)-8-oxoadenine

Guidance literature:: tert-butyl 2-(3-oxopropoxy)acetate; 6-amino-2-(2-methoxyethoxy)-9-(4-((methylamino)methyl)benzyl)-7,9-dihydro-8H-purin-8-one; With sodium tris(acetoxy)borohydride; In 1-methyl-pyrrolidin-2-one; for 15h;

With ammonia; water; In 1-methyl-pyrrolidin-2-one;

Reference yield: 73.0%

: 67-56-1
methanol

: 930294-40-9
9-[4-(3-tert-butoxycarbonylmethoxypropyl)-(methyl)-aminomethylbenzyl]-7,8-dihydro-2-(2-methoxyethoxy)-8-oxoadenine

: 930293-85-9
7,8-dihydro-9-[4-(3-methoxycarbonylmethoxypropyl)(methyl)-aminomethylbenzyl]-2-(2-methoxyethoxy)-8-oxoadenine

Guidance literature:: 9-[4-(3-tert-butoxycarbonylmethoxypropyl)-(methyl)-aminomethylbenzyl]-7,8-dihydro-2-(2-methoxyethoxy)-8-oxoadenine; With hydrogenchloride; In 1,4-dioxane; methanol; chloroform; for 9h; Heating / reflux;

methanol; With sulfuric acid; for 3h; Heating / reflux;

With ammonia; water;