(S)-1-(4-iodo-5-methoxy-2-nitrophenyl)-2,2-dimethyl-1-propyl (1S)-camphanate

Base Information

Chemical Name:(S)-1-(4-iodo-5-methoxy-2-nitrophenyl)-2,2-dimethyl-1-propyl (1S)-camphanate
CAS No.:1427311-75-8
Molecular Formula:C₂₂H₂₈INO₇
Molecular Weight:545.371
Hs Code.:

Synonyms:(S)-1-(4-iodo-5-methoxy-2-nitrophenyl)-2,2-dimethyl-1-propyl (1S)-camphanate

Suppliers and Price of (S)-1-(4-iodo-5-methoxy-2-nitrophenyl)-2,2-dimethyl-1-propyl (1S)-camphanate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-1-(4-iodo-5-methoxy-2-nitrophenyl)-2,2-dimethyl-1-propyl (1S)-camphanate

Chemical Property:

Purity/Quality:

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Technology Process of (S)-1-(4-iodo-5-methoxy-2-nitrophenyl)-2,2-dimethyl-1-propyl (1S)-camphanate

There total 4 articles about (S)-1-(4-iodo-5-methoxy-2-nitrophenyl)-2,2-dimethyl-1-propyl (1S)-camphanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: (R/S)-1-(4-iodo-5-methoxy-2-nitrophenyl)-2,2-dimethyl-1-propyl (1S)-camphanate

: 1427311-74-7
(R)-1-(4-iodo-5-methoxy-2-nitrophenyl)-2,2-dimethyl-1-propyl (1S)-camphanate

: 1427311-75-8
(S)-1-(4-iodo-5-methoxy-2-nitrophenyl)-2,2-dimethyl-1-propyl (1S)-camphanate

Guidance literature:: In ethanol; Reflux;

Reference yield:

: 766-85-8
3-methoxy-1-iodobenzene

: 1427311-75-8
(S)-1-(4-iodo-5-methoxy-2-nitrophenyl)-2,2-dimethyl-1-propyl (1S)-camphanate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium nitrite; acetic acid; nitric acid / 24 h / 20 °C

1.2: 60 °C

2.1: phenylmagnesium chloride / tetrahydrofuran / 2 h / -40 °C / Inert atmosphere

2.2: 3 h / -30 - 20 °C / Inert atmosphere

2.3: Inert atmosphere

3.1: dmap / dichloromethane / 20 °C / Inert atmosphere

4.1: ethanol / Reflux

With dmap; phenylmagnesium chloride; nitric acid; acetic acid; sodium nitrite; In tetrahydrofuran; ethanol; dichloromethane;

Reference yield:

: 55215-55-9
1,4-diiodo-2-methoxy-5-nitrobenzene

: 1427311-75-8
(S)-1-(4-iodo-5-methoxy-2-nitrophenyl)-2,2-dimethyl-1-propyl (1S)-camphanate

Guidance literature:: Multi-step reaction with 3 steps

1.1: phenylmagnesium chloride / tetrahydrofuran / 2 h / -40 °C / Inert atmosphere

1.2: 3 h / -30 - 20 °C / Inert atmosphere

1.3: Inert atmosphere

2.1: dmap / dichloromethane / 20 °C / Inert atmosphere

3.1: ethanol / Reflux

With dmap; phenylmagnesium chloride; In tetrahydrofuran; ethanol; dichloromethane;